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黔江区桑叶中重金属污染及农药残留现状分析与评价

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目的 对重庆市黔江区桑叶中5种重金属污染和42种农药残留进行测定,为辖区内蚕桑业的发展、桑叶类药食产品的质量安全控制提供参考依据.方法 从黔江区内4个片区共采集196批样品,采用电感耦合等离子体质谱法、气相色谱-质谱法进行重金属及农药残留的测定,用内梅罗污染指数法、单因子污染指数法等方法综合评价重金属污染及农药残留风险.结果 196批次桑叶样品中,共检出重金属196批次,检出率100%,污染类型为复合型重金属污染,其中铬(Cr)检出率最高,为96.94%,铅(Pb)次之,Cd(镉)未检出.选取其中154批桑叶进行农药残留检测,检出农药残留样品55批次,检出率为35.71%;42种农残项目中检出12种,其中毒死蜱、敌敌畏检出频次较高;不同乡镇片区之间及不同月份检出情况存在极显著差异(P<0.01),金溪片区检出数及检出率最高.结论 部分乡镇农药使用情况较为普遍,重金属含量偏高,过量食用可能会存在一定风险,需引起相关部门注意.
Analysis and Evaluation of Heavy Metal Pollution and Pesticide Residues in Mulberry Leaves in Qianjiang District
Objective To determine the contamination of 5 heavy metals and 42 pesticide residues in mulberry leaves in Qianjiang District of Chongqing City,so as to provide reference for the development of sericulture industry and the quality and safety control of mulberry leaves products.Methods Total 196 lots of samples were collected from four areas of Qianjiang District.Inductively coupled plasma mass spectrometry(ICP-MS)and gas chromatography-mass spectrometry(GC-MS)were used for the determination of heavy metals and pesticide residues.Nemerow pollution index(NCI)and single factor pollution index(NCI)were used to evaluate the risk of heavy metals and pesticide residues.Results Among 196 batches of mulberry leaf samples,196 batches of heavy metals were detected and the detection rate was 100%.The type of pollution was compound heavy metal pollution,and the highest detection rate was 96.94%for chromium(Cr)followed by lead(Pb),but cadmium(Cd)was not detected.Among them,154 batches of mulberry leaves samples were selected for pesticide residue detection,55 batches of pesticide residue were detected,and the detection rate was 35.71%.Among 42 kinds of pesticide residues,12 species were detected,among which chlorpyrifos and dichlorvos were detected more frequently.There were significant differences between the detection rates of different towns and different months(P<0.01),and the number and detection rate of Jinxi area were the top.Conclusion The use of pesticide is common in some villages and towns,and high heavy metal content and excessive consumption may have certain risks,which should be paid attention by relevant authorities.

mulberry leafheavy metalpesticide residueanalysis and evaluation

王春林、田霞、赵光铃、肖陈、余为、田毅

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重庆市黔江食品药品检验所,重庆 409000

桑叶 重金属 农药残留 分析与评价

黔江区科技计划项目

黔科计2021070

2024

食品与药品
山东省生物药物研究院

食品与药品

CSTPCD
影响因子:0.537
ISSN:1672-979X
年,卷(期):2024.26(1)
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