首页|牛白藤红外指纹图谱研究

牛白藤红外指纹图谱研究

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目的 探索牛白藤红外光谱(IR)快速鉴定技术.方法 采用傅里叶变换红外光谱(FT-IR)对牛白藤原药材进行整体分析.结果 获得牛白藤的红外指纹图谱特征吸收峰有:3418,2925,2854,1723,1650,1514,1401,1319,1267,1155,1104,1054,1030,919,811,782,763,664,592,538,520 cm-1,并确定1267,1030,919 cm-1为牛白藤镇痛抗炎药效成分熊果酸的红外特征指示峰.各样品IR相似度在0.9003~0.9895范围内,因此拟定牛白藤的IR相似度阈值为0.90.结论 牛白藤的FT-IR指纹图谱可为其快速鉴定及质量控制提供科学依据.
Study on Infrared Fingerprinting of Hedyotis Hedyotidea(DC.)Merr.
Objective To explore the rapid identification technology of Hedyotis hedyotidea(DC.)Merr.by infrared spectroscopy(IR).Methods The overall analysis of the medicinal materials of Hedyotis hedyotidea(DC.)Merr.was performed by FT-IR.Results The characteristic absorption peaks of IR fingerprint of Hedyotis hedyotidea(DC.)Merr.were obtained as follows:3418,2925,2854,1723,1650,1514,1401,1319,1267,1155,1104,1054,1030,919,811,782,763,664,592,538,520 cm-1.1267,1030 cm-1 and 919 cm-1 were the IR characteristic indicative peaks of ursolic acid,which was one of the analgesic and anti-inflammatory components of Hedyotis hedyotidea(DC.)Merr..The IR similarity among the samples was in the range of 0.9003-0.9895,thus the IR similarity threshold of Hedyotis hedyotidea(DC.)Merr.was proposed as 0.90.Conclusion The FT-IR fingerprint of Hedyotis hedyotidea(DC.)Merr.can provide scientific basis for its rapid identification and quality control.

Hedyotis hedyotidea(DC.)Merr.FT-IRfingerprint

银胜高、陈燕燕、陈诗曼、岑燕霞、陆海琳

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广西中医药大学,广西 南宁 530000

牛白藤 傅里叶变换红外光谱 指纹图谱

广西自然科学基金项目广西中医药大学2019~2021年广西一流学科建设开放课题

2017GXNSFAA1983162019XK096

2024

食品与药品
山东省生物药物研究院

食品与药品

CSTPCD
影响因子:0.537
ISSN:1672-979X
年,卷(期):2024.26(2)
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