食品与药品2024,Vol.26Issue(2) :144-147.DOI:10.3969/j.issn.1672-979X.2024.02.008

牛白藤红外指纹图谱研究

Study on Infrared Fingerprinting of Hedyotis Hedyotidea(DC.)Merr.

银胜高 陈燕燕 陈诗曼 岑燕霞 陆海琳
食品与药品2024,Vol.26Issue(2) :144-147.DOI:10.3969/j.issn.1672-979X.2024.02.008

牛白藤红外指纹图谱研究

Study on Infrared Fingerprinting of Hedyotis Hedyotidea(DC.)Merr.

银胜高 1陈燕燕 1陈诗曼 1岑燕霞 1陆海琳1
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作者信息

  • 1. 广西中医药大学,广西 南宁 530000
  • 折叠

摘要

目的 探索牛白藤红外光谱(IR)快速鉴定技术.方法 采用傅里叶变换红外光谱(FT-IR)对牛白藤原药材进行整体分析.结果 获得牛白藤的红外指纹图谱特征吸收峰有:3418,2925,2854,1723,1650,1514,1401,1319,1267,1155,1104,1054,1030,919,811,782,763,664,592,538,520 cm-1,并确定1267,1030,919 cm-1为牛白藤镇痛抗炎药效成分熊果酸的红外特征指示峰.各样品IR相似度在0.9003~0.9895范围内,因此拟定牛白藤的IR相似度阈值为0.90.结论 牛白藤的FT-IR指纹图谱可为其快速鉴定及质量控制提供科学依据.

Abstract

Objective To explore the rapid identification technology of Hedyotis hedyotidea(DC.)Merr.by infrared spectroscopy(IR).Methods The overall analysis of the medicinal materials of Hedyotis hedyotidea(DC.)Merr.was performed by FT-IR.Results The characteristic absorption peaks of IR fingerprint of Hedyotis hedyotidea(DC.)Merr.were obtained as follows:3418,2925,2854,1723,1650,1514,1401,1319,1267,1155,1104,1054,1030,919,811,782,763,664,592,538,520 cm-1.1267,1030 cm-1 and 919 cm-1 were the IR characteristic indicative peaks of ursolic acid,which was one of the analgesic and anti-inflammatory components of Hedyotis hedyotidea(DC.)Merr..The IR similarity among the samples was in the range of 0.9003-0.9895,thus the IR similarity threshold of Hedyotis hedyotidea(DC.)Merr.was proposed as 0.90.Conclusion The FT-IR fingerprint of Hedyotis hedyotidea(DC.)Merr.can provide scientific basis for its rapid identification and quality control.

关键词

牛白藤/傅里叶变换红外光谱/指纹图谱

Key words

Hedyotis hedyotidea(DC.)Merr./FT-IR/fingerprint

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基金项目

广西自然科学基金项目(2017GXNSFAA198316)

广西中医药大学2019~2021年广西一流学科建设开放课题(2019XK096)

出版年

2024
食品与药品
山东省生物药物研究院

食品与药品

CSTPCD
影响因子:0.537
ISSN:1672-979X
参考文献量21
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