易混淆中药地骨皮、香加皮、五加皮鉴别研究

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中文摘要：目的:探讨区分鉴别易混淆皮类中药地骨皮、香加皮、五加皮的方法.方法:采用性状、微性状、显微、荧光鉴别等方法对地骨皮、香加皮、五加皮进行鉴别研究.结果:地骨皮、香加皮、五加皮在性状和微性状方面的主要鉴别点是外表面、断面和气味;显微鉴别的重点是草酸钙结晶不同.传统荧光法在紫外灯下观察三者的荧光现象区别不明显,但是二维荧光和三维荧光等方面均有较大差异.二维荧光光谱结果显示,三种药材的水提取液均只有一个荧光峰,三者的峰位、峰强度和峰形有很大差别;三维荧光光谱结果显示,地骨皮有三个荧光峰,香加皮和五加皮有两个荧光峰,三者的峰位和峰强度有明显差异.结论:传统鉴别方法可用于地骨皮、香加皮、五加皮的鉴别,二维荧光光谱法和三维荧光光谱法可快速、准确地区分三种药材.

外文标题：Identification Study on Easily Confusing Chinese Medicinals of Digupi(Lycii Cortex),Xiangjiapi(Periplocae Cortex)and Wujiapi(Acanthopanacis Cortex)

外文摘要：Objective:To investigate the methods for distinguishing and identifying the easily confusing Chinese medicinal cortex:Digupi(Lycii Cortex),Xiangjiapi(Periplocae Cortex)and Wujiapi(Acanthopanacis Cortex).Methods:The identification of Digupi,Xiangjiapi and Wujiapi were studied by traits,micro-traits,microscopy and fluorescence identification.Results:The main identification points of Digupi,Xiangjiapi and Wujiapi in terms of traits and micro-traits are the external surface,section and odor.The focus of microscopic identification is the different crystalliza-tion of calcium oxalate.The fluorescence phenomenon of the three herbs observed by traditional fluorescence method under ultraviolet lamp were not significantly different,but there were great differences in two-dimensional fluorescence and three-dimensional fluorescence.The results of two-dimensional fluorescence spectrum showed that there was only one fluorescence peak in the water extract of the three medicinal materials,and the peak position,peak intensity and peak shape of the three medicinal materials were very different.The results of three-dimensional fluorescence spectrum showed that there were three fluorescence peaks in Digupi,two fluorescence peaks in Xiangjiapi and Wujiapi,and the peak position and peak intensity of the three medicinal materials were significantly different.Conclusions:The traditional identification methods can be used for the identification of Digupi,Xiangjiapi and Wujiapi.Two-dimensional fluorescence spectroscopy and three-dimensional fluorescence spectroscopy can quickly and accurately distinguish the three medicinal materials.

外文关键词：

Digupi(Lycii Cortex)Xiangjiapi(Periplocae Cortex)Wujiapi(Acanthopanacis Cortex)micro-trait identification methodtwo-dimensional fluorescence spectroscopythree-dimensional fluorescence spectroscopy

作者：

秦露、吕绪桢、刘亚丽、赵天伦、王晨曦、战瑞雪、冯帅、李峰

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作者单位：

山东中医药大学,山东济南 250355

山东省高校中药质量控制与全产业链建设协同创新中心,山东济南 250355

关键词：

地骨皮香加皮五加皮微性状鉴别法二维荧光光谱法三维荧光光谱法

基金：

国家科技重大专项山东省医药卫生科技发展计划项目山东省高校中药质量控制与全产业链建设协同创新中心项目2022年全国名老中医药专家传承工作室建设项目

项目编号：

2017ZX09301058202013030996CYLXTCX2021-08国中医药人教函[2022]75号

出版年：

2024

DOI：

10.16294/j.cnki.1007-659x.2024.01.015

山东中医药大学学报

山东中医药大学

山东中医药大学学报

CSTPCD

影响因子：0.52

ISSN：1007-659X

年,卷(期)：2024.48(1)

参考文献量25