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不同柑橘属水果果皮中萜烯含量测定与分析

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本研究建立了气相色谱-质谱联用(Gas Chromatography-Mass Spectrometry,GC-MS)分离测定果皮中 12 种萜烯类物质的方法,以 15 mL甲醇为溶剂、使用水浴恒温振荡器萃取 60 min时萃取效果最佳.12 种萜烯的回收率在74.6%~122.5%,检出限在 0.004~2.190 mg·L-1,精密度较好.16种柑橘属水果果皮中柠檬烯含量最高,且萜烯含量受水果产地、种类等因素的影响,此方法可用于产地溯源.
Determination and Analysis of Terpene Content in the Peels of Different Citrus Fruits
This study established a detection method based on gas chromatography-mass spectrometry(GC-MS)to extract and quantify 12 terpenes in fruit peels.The extraction effect was the best when 15 mL methanol was used as solvent and water bath constant temperature oscillator was used to extract 60 min.The recovery of 12 terpenes was 74.6%~122.5%,and the limit of detection was 0.004~2.190 mg·L-1.The content of limonene in the peel of 16 Citrus fruits was the highest,and the content of terpenes was affected by factors such as fruit origin and species.This method can be used for origin traceability.

Citrus fruitsterpenegas chromatography-mass spectrometrypericarp

姚力文、蒋薇、司晓喜、张凤梅、陕绍云

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昆明理工大学 化学工程学院,云南昆明 650500

云南中烟工业有限责任公司技术中心 云南烟草化学重点实验室,云南昆明 650231

柑橘属水果 萜烯 气相色谱-质谱联用 果皮

云南省科技厅技术创新人才培养对象项目云南中烟工业有限责任公司科技项目云南中烟人才项目国家自然科学基金

202405AD3500182023YJ01滇烟工人[2021]293号22068023

2024

食品安全导刊
商业科技质量中心 北京肉类食品协会

食品安全导刊

影响因子:0.065
ISSN:1674-0270
年,卷(期):2024.(2)
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