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海南热带水果芒果重金属含量特征分析

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目的:了解海南热带水果芒果中重金属含量特征以及受污染程度.方法:采用微波消解-电感耦合等离子体质谱技术对海南热带水果芒果中重金属的含量进行检测,然后采用污染指数对其受污染程度进行评价分析.结果:建立的检测方法在0~50 μg·L-1 线性关系良好,相关系数大于0.995;在加标水平为5 μg·mL-1时,回收率为 91.2%~108.0%,RSD为 0.14%~4.53%.芒果中重金属含量变化范围较宽,重金属Cu平均含量最高,为 2.72 mg·kg-1,Hg和As未检出.结论:所建立的方法精密度高,操作简单、快速,可同时测定芒果中多种重金属含量.所测芒果样品重金属含量均低于相应的规定限值,没有超标现象,属于清洁安全食品.
Analysis of Heavy Metal Content Characteristics of Tropical Fruit Mangoes in Hainan
Objective:To understand the characteristics of heavy metal content and pollution level in tropical fruit mangoes in Hainan.Method:The contents of eight heavy metals in Hainan tropical fruits and mangoes were determined by microwave-inductively coupled plasma mass spectrometry(MD-ICP-MS).Then the pollution index is used to evaluate the pollution degree.Result:The established method showed good linearity in the concentration range of 0~50 μg·L-1 with the correlation coefficients greater than 0.995.The recoveries ranged from 91.2%to 108.0%at the spiked level of 5 μg·mL-1,and the RSD were from 0.14%to 4.53%.The heavy metal contents in mango varied over a wide range,with the highest average content of heavy metal Cu at 2.72 mg·kg-1,and Hg and As were not detected.Conclusion:The established method has high precision,simple and rapid operation,and can be used for the simultaneous determination of various heavy metals in mango.The heavy metal contents of the measured mango samples were lower than the corresponding prescribed limits and did not exceed the limits,which are clean and safe foods.

mangoesmicrowave digestion-inductively coupled plasma mass spectrometryheavy metalpollution index

梁琼、张玉霞、林树秀、谷满屯

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海南省检验检测研究院,海南海口 570311

海南省工商职业学院,海南海口 570203

海南省食品检验检测中心(海南省实验动物中心),国家市场监管重点实验室(热带果蔬质量与安全),海南海口 570314

芒果 微波消解-电感耦合等离子体质谱 重金属 污染指数

国家市场监管重点实验室(热带果蔬质量与安全)基础应用研究课题

KF-2023015

2024

食品安全导刊
商业科技质量中心 北京肉类食品协会

食品安全导刊

影响因子:0.065
ISSN:1674-0270
年,卷(期):2024.(7)
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