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基于LC-MS/MS的蔬菜农药残留基质效应分析

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为明确蔬菜农药残留对于基质效应的影响,本文选取韭菜、芹菜、茄子3种蔬菜,利用液相色谱-串联质谱法对蔬菜中 6 种农药残留进行测定,通过基质和溶剂标准曲线的斜率,判定其基质效应.试验结果表明,不同蔬菜中农药残留量的基质效应主要为信号抑制作用.因此,在后期农药检测中,可通过使用基质标准曲线进行定量测定,从而提高检测结果的准确性,对于保障食品安全具有重要意义.
Matrix Effect Analysis of Vegetable Pesticide Residues Based on LC-MS/MS
In order to clarify the influence of pesticide residues in vegetables on the matrix effect,three kinds of vegetables,leek,celery and eggplant,were selected in this paper.The six pesticide residues in vegetables were determined by liquid chromatography-tandem mass spectrometry.The matrix effect was determined by the slope of the matrix and solvent standard curve.The results showed that the matrix effect of pesticide residues in different vegetables was mainly signal inhibition.Therefore,in the later pesticide detection,the matrix standard curve can be used for quantitative determination,so as to improve the accuracy of the test results,which is of great significance for ensuring food safety.

LC-MS/MSvegetable pesticide residuesmatrix effect

单晓丽、周峰、李东、王国洋

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安丘市检验检测中心有限公司,山东潍坊 262100

山东柠檬生化有限公司,山东潍坊 262100

LC-MS/MS 蔬菜农药残留 基质效应

2024

食品安全导刊
商业科技质量中心 北京肉类食品协会

食品安全导刊

影响因子:0.065
ISSN:1674-0270
年,卷(期):2024.(7)
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