食品安全导刊2024,Issue(7) :93-95,99.

微波消解-原子荧光光谱法测定栀子中硒含量

Determination on Selenium in Gardenia by Microwave Digestion-Atomic Fluorescence Spectrometry Method

陈思 王姣
食品安全导刊2024,Issue(7) :93-95,99.

微波消解-原子荧光光谱法测定栀子中硒含量

Determination on Selenium in Gardenia by Microwave Digestion-Atomic Fluorescence Spectrometry Method

陈思 1王姣1
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作者信息

  • 1. 湘潭医卫职业技术学院,湖南湘潭 411102
  • 折叠

摘要

本文采用微波消解-原子荧光光谱法测定栀子中的硒元素含量.结果表明,使用 8 mL硝酸和2 mL过氧化氢时,能够将 0.300 0 g的栀子样品完全消解,并且荧光强度良好.方法在 0~10 μg·L-1 具有良好的线性关系,检出限为 0.050 5 ng·mL-1,精密度为 3.0%,加标回收率在 96.80%~100.34%.该方法具有较高的准确性和灵敏度.

Abstract

The content of selenium in gardenia jasminoides was determined by microwave digestion and atomic fluorescence spectrometry.The results showed that 0.300 0 g of gardenia samples could be completely dissolved with 8 mL of nitric acid and 2 mL of hydrogen peroxide,and the fluorescence intensity was good.The detection limit was 0.050 5 ng·mL-1,the precision was 3.0%,and the recoveries were 96.80%~100.34%.The method has high accuracy and sensitivity.

关键词

微波消解法/原子荧光光谱法/

Key words

microwave digestion method/atomic fluorescence spectrometry/selenium

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基金项目

湘潭市科技局指导项目(CG-ZDJH-202139)

出版年

2024
食品安全导刊
商业科技质量中心 北京肉类食品协会

食品安全导刊

影响因子:0.065
ISSN:1674-0270
参考文献量9
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