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高效液相色谱法测定饮料中8种人工合成着色剂的含量

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建立了固相萃取法结合高效液相色谱法测定饮料中8 种着色剂含量的方法.结果表明,8 种着色剂在0.5~50.0 μg·mL-1 浓度范围内线性关系良好,相关系数均大于0.999;精密度实验RSD在0.7%~2.2%;平均加标回收率为91.67%~93.79%,RSD≤3.8%.对20批不同类型饮料中8种人工合成着色剂进行测定,结果显示饮料中色素均未超出规定限值.本方法简便、高效,可用于同时测定饮料中8种人工合成着色剂.
Determination of 8 Synthetic Colorants in Beverages by High Performance Liquid Chromatography
A method for the determination of eight colorants in beverages by solid-phase extraction coupled with high performance liquid chromatography(HPLC)was established.The results showed that the linearity of the eight colorants was good in the concentration range of 0.5~50.0 μg·mL-1 with the correlation coefficients greater than 0.999;the RSD of the precision experiments were in the range of 0.7%~2.2%;and the average spiked recoveries were in the range of 91.67%~93.79%with the RSD≤3.8%.Eight artificial colorants in 20 batches of different types of beverages were measured,and the results showed that none of the pigments in the beverages exceeded the prescribed limit.This method is simple and efficient,and can be used for the simultaneous determination of 8 synthetic colorants in beverages.

beveragehigh performance liquid chromatographysynthetic colorant

郭璞

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运城市综合检验检测中心,山西运城 044000

饮料 高效液相色谱法 人工合成着色剂

2024

食品安全导刊
商业科技质量中心 北京肉类食品协会

食品安全导刊

影响因子:0.065
ISSN:1674-0270
年,卷(期):2024.(9)
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