食品安全导刊2024，Issue(9) ：111-113,117.

基于GC-MS/MS技术对承德地区山楂中44种农药残留分析评价

Analysis and Evaluation of 44 Pesticide Residues in Crataegus pinnatifida Bge.in Chengde Area Based on GC-MS/MS Technology

杨爽 袁婧威 杜培楠 张波 庞婕 高婧
食品安全导刊2024，Issue(9) ：111-113,117.
✕
  • 维普
  • 万方数据

基于GC-MS/MS技术对承德地区山楂中44种农药残留分析评价

Analysis and Evaluation of 44 Pesticide Residues in Crataegus pinnatifida Bge.in Chengde Area Based on GC-MS/MS Technology

杨爽 1袁婧威 1杜培楠 1张波 1庞婕 1高婧1
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作者信息

  • 1. 承德市食品药品检验检测中心,河北承德 067001
  • 折叠

摘要

目的:对承德地区山楂中 44 种农药残留进行检测分析并评价.方法:利用气相色谱-质谱/质谱联用方法检测山楂样品中44种农药残留含量.结果:44种农药残留组分在0.2～0.6 μg·mL-1 线性关系良好,相关系数均大于 0.998,加标回收率在 70.8%～104.5%,相对标准偏差在 0.18%～5.20%.结论:承德地区山楂产品安全性较高,病虫害综合防治技术较好,能够为食品安全监管提供数据支持.

Abstract

Objective:To detect and evaluate 44 kinds of pesticide residues in Crataegus pinnatifida Bge.in Chengde area.Method:44 pesticide residues in Crataegus pinnatifida Bge.samples were determined by gas chromatography-mass spectrometry.Result:The 44 pesticide residues had a good linear relationship between 0.2 μg·mL-1 and 0.6 μg·mL-1,the correlation coefficients were greater than 0.998,the recoveries were 70.8%～104.5%,and the relative standard deviation was 0.18%～5.20%.Conclusion:The safety of hawthorn products in Chengde area is high,and the comprehensive control technology of pest and disease is good,which can provide data support for food safety supervision.

关键词

气相色谱-质谱/质谱联用/山楂/农药残留

Key words

gas chromatography-mass/mass spectrometry/Crataegus pinnatifida Bge./pesticide residues

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出版年

2024
食品安全导刊
商业科技质量中心 北京肉类食品协会

食品安全导刊

影响因子：0.065
ISSN：1674-0270
参考文献量5
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