首页|HPLC-柱后光化学衍生法检测芝麻酱中黄曲霉毒素B1

HPLC-柱后光化学衍生法检测芝麻酱中黄曲霉毒素B1

扫码查看
本文建立了HPLC-柱后光化学衍生-荧光检测器测定芝麻酱中黄曲霉毒素B1 的方法.结果表明,黄曲霉毒素B1 在 0.077 4~1.934 5 ng·mL-1 线性关系良好,线性系数为 0.999 9,加标回收率为100.81%~105.46%,相对标准偏差为 0.48%,定量限为0.029 μg·kg-1,检出限为0.01 μg·kg-1.该方法的前处理过程简单方便,结果准确,可用于芝麻酱中黄曲霉毒素B1 的批量快速检测.
Determination of Aflatoxin B1 in Sesame Paste by HPLC-Post-Column Photochemical Derivatization
A method for the determination of aflatoxins B1 in tahini paste by HPLC-post column photochemical derivation-fluorescence detector was developed.The results showed that aflatoxins B1 had a good linear relationship between 0.077 4 ng·mL-1 and 1.934 5 ng·mL-1,the linear coefficient was 0.999 9,the standard recovery was 100.81%~105.46%,relative standard deviation was 0.48%,and the limit of quantition was 0.029 μg·kg-1.The detection limit was 0.01 μg·kg-1.The pretreatment process of this method is simple and convenient,the result is accurate,and it can be used for batch rapid detection of aflatoxin B1 in tahini paste.

high performance liquid chromatographyaflatoxin B1Sesame paste

李二冬

展开 >

山西省检验检测中心(山西省标准计量技术研究院),山西太原 030032

高效液相色谱法 黄曲霉毒素B1 芝麻酱

山西省青年科学研究项目

202203021212443

2024

食品安全导刊
商业科技质量中心 北京肉类食品协会

食品安全导刊

影响因子:0.065
ISSN:1674-0270
年,卷(期):2024.(12)
  • 10