首页|液相色谱串联质谱法测定鸡蛋中金刚乙胺残留量的研究

液相色谱串联质谱法测定鸡蛋中金刚乙胺残留量的研究

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目的:建立液相色谱串联质谱法测定鸡蛋中金刚乙胺残留量的分析方法,为鸡蛋食品安全检测工作提供技术支持.方法:采用液相色谱串联质谱法测定鸡蛋中金刚乙胺的残留量.结果:在质量浓度为1~20 ng·mL-1,金刚乙胺的线性关系良好,相关系数为0.9998,回收率为84.3%~91.6%,定量限为1 μg·kg-1.结论:该方法检测效果良好,可以应用于鸡蛋中金刚乙胺含量的实际监测工作中.
Study on the Determination of Residual Amantadine in Eggs by Liquid Chromatography Tandem Mass Spectrometry
Objective:To establish an analytical method for the determination of rimantadine residue in eggs by liquid chromatography-tandem mass spectrometry,and to provide technical support for the detection of egg food safety.Method:The residue of rimantadine in eggs was determined by liquid chromatography-tandem mass spectrometry.Result:The linear relationship of rimantadine was good at the mass concentration of 1~20 ng·mL-1,the correlation coefficient was 0.9998,the recovery was 84.3%~91.6%,and the limit of quantitation was 1 μg·kg-1.Conclusion:The method has good detection effect and can be applied to the actual monitoring of rimantadine content in eggs.

liquid chromatography tandem mass spectrometryeggsmatrix effectdiamond ethylamine

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安徽省淮北市濉溪县市场监督检验所,安徽淮北 235199

液相色谱串联质谱法 鸡蛋 基质效应 金刚乙胺

2024

食品安全导刊
商业科技质量中心 北京肉类食品协会

食品安全导刊

影响因子:0.065
ISSN:1674-0270
年,卷(期):2024.(15)