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火焰原子吸收光谱法测定玻璃制品中铅、镉迁移量

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目的:建立火焰原子吸收光谱法同时测定玻璃制品中铅、镉迁移量的分析方法.方法:玻璃制品试样经清洗晾干,注入4%乙酸溶液,于22℃下进行24 h迁移试验,浸泡液供原子吸收分光光度计测定.结果:铅、镉两种元素在各自线性范围内线性关系良好,检出限分别为0.07 mg·L-1、0.007 mg·L-1,加标回收率在 92.0%~104.5%,相对标准偏差≤3.82%.结论:该方法操作简便、准确快速,适用于食品接触用玻璃制品中铅、镉迁移量的批量分析检测.
Determination of Plumbum and Cadmium Migration in Glass Products by Flame Atomic Absorption Spectrometry
Objective:An analytical method for simultaneous determination of plumbum and cadmium migration in glass products by flame atomic absorption spectrometry was established.Method:The glass samples were washed and dried,injected with 4%acetic acid solution,and carried out migration test at 22℃for 24 h.The soaked solution was used for the determination by atomic absorption spectrophotometer.Result:The detection limits of plumbum and cadmium were 0.07 mg·L-1 and 0.007 mg·L-1,respectively.The recoveries of plumbum and cadmium were between 92.0%and 104.5%,and the relative standard deviation was less than 3.82%.Conclusion:The method is simple,accurate and rapid,and is suitable for batch analysis and detection of plumbum and cadmium migration in glass products for food contact.

flame atomic absorption spectroscopyglasswareplumbumcadmium

苏崯、王永卿、张莎

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祁县综合检验检测中心(国家玻璃器皿产品质量监督检验中心),山西晋中 030900

原子吸收光谱法 玻璃制品

2024

食品安全导刊
商业科技质量中心 北京肉类食品协会

食品安全导刊

影响因子:0.065
ISSN:1674-0270
年,卷(期):2024.(16)
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