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气相色谱法测定蔬菜中多种有机磷农药残留

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通过优化进样量、进样方式、温度程序和梯度设置等检测条件,建立了一种高效、可靠的气相色谱法检测蔬菜中多种有机磷农药残留的方法.实验结果显示,各有机磷农药在 0.025~10.000 μg·mL-1 具有良好线性关系,相关系数均大于 0.999.加标回收率均在 80%以上,相对标准偏差均小于 5%.该方法具有较高的灵敏度、较好的准确性和重复性,可有效应用于蔬菜中有机磷农药残留的检测,为食品安全提供可靠的技术支持.
Determination of Organophosphorus Pesticide Residues in Vegetables by Gas Chromatography
By optimizing the detection conditions such as injection volume,injection mode,temperature program and gradient setting,an efficient and reliable gas chromatography method for the detection of various organophosphorus pesticide residues in vegetables was established.The experimental results showed that the organophosphorus pesticides had a good linear relationship in the range of 0.025~10.00 μg·mL-1,with correlation coefficients greater than 0.999.The recovery rate of spiked samples is above 80%,and the relative standard deviation is less than 5% .This method has high sensitivity,accuracy and repeatability,and can be effectively applied to the detection of organophosphorus pesticide residues in vegetables,providing reliable technical support for food safety.

gas chromatographyvegetablesorganophosphorus pesticide residuesfood safety

吴少青、戴立红、黄浩峰、徐奕晖、苏晓濛、赵颖峰

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南京市产品质量监督检验院(南京市质量发展与先进技术应用研究院),江苏南京 210000

气相色谱 蔬菜 有机磷农药残留 食品安全

2024

食品安全导刊
商业科技质量中心 北京肉类食品协会

食品安全导刊

影响因子:0.065
ISSN:1674-0270
年,卷(期):2024.(24)