首页|等度离子色谱法同时测定饮用水中4种消毒副产物

等度离子色谱法同时测定饮用水中4种消毒副产物

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目的:建立饮用水中亚氯酸盐、氯酸盐、二氯乙酸及三氯乙酸的离子色谱检测方法.方法:水样经0.22 µm滤膜过滤,使用DIONEX ICS-900离子色谱仪检测,6 mmol·L-1 KOH等度洗脱,保留时间定性,外标法定量.结果:该方法线性关系良好(r>0.997),精密度高(相对标准偏差<10%),样品加标平均回收率为 80.6%~115.3%.结论:该方法操作快捷、简单高效,用OH-作为淋洗液可以降低背景噪音,使得低含量的消毒副产物检测结果更加准确、可靠.
Simultaneous Determination of Four Disinfection By-Products in Drinking Water by Plasma Chromatography
Objective:To establish ion chromatography method for the detection of chlorite,chlorate,dichloroacetic acid and trichloroacetic acid in drinking water.Method:The water samples were filtered through a 0.22 μm aqueous membrane,and then tested by DIONEX ICS-900 ion chromatograph,6 mmol·L-1 KOH was eluted isocracies,retention time was qualitative,and external standard method was quantified.Result:The method had a good linear relationship(r>0.997),high precision(relative standard deviation less than 10%),and the average recovery rate of samples spiked was 80.6%to 115.3%.Conclusion:The method is fast,simple and efficient.At the same time,OH-is used as the eluent,which can reduce the background noise,so that the detection results of low-level disinfection by-products are more accurate and reliable.

equivalention chromatographydrinking waterdisinfection by-products

罗玉琴、李华冰、莫勤妹

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崇左市疾病预防控制中心,广西崇左 532200

崇左市食品药品检验所,广西崇左 532200

崇左市农业综合检测中心,广西崇左 532200

等度 离子色谱法 饮用水 消毒副产物

2024

食品安全导刊
商业科技质量中心 北京肉类食品协会

食品安全导刊

影响因子:0.065
ISSN:1674-0270
年,卷(期):2024.(28)
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