首页|固相萃取-液相色谱串联质谱法测定婴儿食品中的4种添加剂

固相萃取-液相色谱串联质谱法测定婴儿食品中的4种添加剂

Determination of Four Additives in Infant Food by Solid Phase Extraction-Liquid Chromatography-Tandem Mass Spectrometry

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本文建立了一种测定婴儿食品中 4 种常用食品添加剂(香豆素、香草醛、甲基香草醛和乙基香草醛)的方法.结果表明,各目标物质的质量浓度在 50~5 000 ng·mL-1 时线性关系良好,检测限和定量限分别为 10 μg·kg-1 和 50 μg·kg-1;加标浓度为 50 μg·kg-1、100 μg·kg-1、500 μg·kg-1 时,回收率为81.72%~102.13%,相对标准偏差低于10%.说明该方法精准可靠,可用于婴儿食品基质中常见添加剂的检测.
In this paper,a method for the determination of four commonly used food additives(coumarin,vanillin,methylvanillin and ethyl vanillin)in infant food was established.The results showed that the mass concentration of each target substance had a good linear relationship at 50 ng·mL-1 to 5 000 ng·mL-1,and the detection limit and quantification limit were 10 μg·kg-1 and 50 μg·kg-1,respectively.When the spike concentration was 50 μg·kg-1,100 μg·kg-1 and 500 μg·kg-1,the recovery rate was 81.72%to 102.13%,and the relative standard deviation was less than 10%.This method is accurate and reliable,and can be used for the detection of common additives in baby food matrices.

food additivesinfant foodsolid-phase extractionliquid chromatography tandem-mass spectrometry

黄飞

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广东省惠州市质量计量监督检测所,广东 惠州 516000

食品添加剂 婴儿食品 固相萃取 液相色谱串联质谱法

2024

食品安全导刊
商业科技质量中心 北京肉类食品协会

食品安全导刊

影响因子:0.065
ISSN:1674-0270
年,卷(期):2024.(32)