食品安全导刊2024,Issue(32) :71-74.

固相萃取-液相色谱串联质谱法测定婴儿食品中的4种添加剂

Determination of Four Additives in Infant Food by Solid Phase Extraction-Liquid Chromatography-Tandem Mass Spectrometry

黄飞
食品安全导刊2024,Issue(32) :71-74.

固相萃取-液相色谱串联质谱法测定婴儿食品中的4种添加剂

Determination of Four Additives in Infant Food by Solid Phase Extraction-Liquid Chromatography-Tandem Mass Spectrometry

黄飞1
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作者信息

  • 1. 广东省惠州市质量计量监督检测所,广东 惠州 516000
  • 折叠

摘要

本文建立了一种测定婴儿食品中 4 种常用食品添加剂(香豆素、香草醛、甲基香草醛和乙基香草醛)的方法.结果表明,各目标物质的质量浓度在 50~5 000 ng·mL-1 时线性关系良好,检测限和定量限分别为 10 μg·kg-1 和 50 μg·kg-1;加标浓度为 50 μg·kg-1、100 μg·kg-1、500 μg·kg-1 时,回收率为81.72%~102.13%,相对标准偏差低于10%.说明该方法精准可靠,可用于婴儿食品基质中常见添加剂的检测.

Abstract

In this paper,a method for the determination of four commonly used food additives(coumarin,vanillin,methylvanillin and ethyl vanillin)in infant food was established.The results showed that the mass concentration of each target substance had a good linear relationship at 50 ng·mL-1 to 5 000 ng·mL-1,and the detection limit and quantification limit were 10 μg·kg-1 and 50 μg·kg-1,respectively.When the spike concentration was 50 μg·kg-1,100 μg·kg-1 and 500 μg·kg-1,the recovery rate was 81.72%to 102.13%,and the relative standard deviation was less than 10%.This method is accurate and reliable,and can be used for the detection of common additives in baby food matrices.

关键词

食品添加剂/婴儿食品/固相萃取/液相色谱串联质谱法

Key words

food additives/infant food/solid-phase extraction/liquid chromatography tandem-mass spectrometry

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出版年

2024
食品安全导刊
商业科技质量中心 北京肉类食品协会

食品安全导刊

影响因子:0.065
ISSN:1674-0270
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