杞苓氨基酸口服液中枸杞子薄层鉴别方法学研究
Study on Thin-Layer Identification Method of Wolfberry in Qiling Amino Acid Oral Liquid
刘德文 1陈天野 1周彦如 2柳连玉 1邹松 1盛文胜3
作者信息
- 1. 江西德上医药研究院有限公司,江西樟树 331200
- 2. 江西德上制药股份有限公司,江西樟树 331200;江西广来健康产业有限公司,江西樟树 331200
- 3. 江西德上医药研究院有限公司,江西樟树 331200;江西德上制药股份有限公司,江西樟树 331200
- 折叠
摘要
目的:利用薄层色谱(Thin-Layer Chromatography,TLC)鉴别方法确定杞苓氨基酸口服液的特征成分,制订产品控制指标.方法:采用《中华人民共和国药典》(2020 版)薄层色谱法(通则 0502)对主要成分枸杞子进行定性鉴别.结果:枸杞子的薄层色谱斑点清晰可见,在与对照药材相应的位置上,显示相同颜色的荧光斑点,阴性样品无干扰影响.结论:枸杞子鉴别方法操作简便、重复性好、专属性强,检测结果稳定可靠,可作为杞苓氨基酸口服液的质量控制方法之一.
Abstract
Objective:Identifying the characteristic components of Qiling amino acid oral liquid use thin-layer chromatography(TLC)method and establish product control indicators.Method:The thin-layer chromatography method(General Method No.0502 in Pharmacopoeia of China,2020 edition)was used to qualitatively identify the main components of wolfberry.Result:The thin-layer chromatography spots of wolfberry were clearly visible,and the same colored fluorescent spots appeared at the corresponding position with the control herbal materials.No interference was observed in the negative sample.Conclusion:The identification method for wolfberries is easy to operate,good repeatability,strong specificity,and stable and reliable detection results.It can be used as one of the quality control methods for Qiling amino acid oral liquid.
关键词
口服液/薄层鉴别/枸杞子/方法学Key words
oral liquid/thin-layer chromatography/Chinese wolfberry/methodology引用本文复制引用
出版年
2024
NETL
NSTL
万方数据