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ICP-MS法和UV-Vis法测定油炸食品中铝残留量的比较研究

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本文比较电感耦合等离子体质谱法(Inductively Coupled Plasma-Mass Spectrometry,ICP-MS)和紫外可见分光光度法(Ultraviolet-Visible Spectroscopy,UV-Vis)测定油炸食品中铝残留量的线性范围、相关系数、检出限、定量限和准确性,并运用这两种检测方法测定市售油炸食品样品.结果表明,ICP-MS法的线性范围更广、线性更好,检出限、定量限、加标回收率、精密度均优于UV-Vis法.UV-Vis法相比ICP-MS法成本低,但前处理烦琐、耗时、耗试剂、自动化程度低.在日常检测工作中,检测大批量的铝残留量较低的油炸食品更推荐使用ICP-MS法.而为了节约成本,可用UV-Vis法进行添加含铝添加剂的油炸食品中铝残留量的检测.
Comparative Study on Determination of Aluminum Residues in Fried Food by ICP-MS and UV-Vis
In this paper,the linear range,correlation coefficient,detection limit,quantitation limit and accuracy of aluminum residue in fried food were compared by inductively coupled plasma-mass spectrometry(ICP-MS)and ultraviolet-visible spectroscopy(UV-Vis)and the two methods were used to determine the fried food samples.The results show that ICP-MS method has wider linear range,better linear range,detection limit,limit of quantitation,recovery rate and precision than UV-Vis method.Compared with ICP-MS,UV-Vis method has low cost,but the pretreatment is cumbersome,time consuming,reagent consuming and low degree of automation.In daily testing work,it is recommended to use ICP-MS method to detect large quantities of deep-fried food with low aluminum residue.In order to save cost,UV-Vis method can be used to detect residual aluminum in fried food with aluminum additives.

aluminum residuefried foodinductively coupled plasma mass spectrometry(ICP-MS)

林起辉、张建莹、林妮、李俊玉、潘清、谢宗良

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深圳海关食品检验检验技术中心,广东 深圳 518000

铝残留量 油炸食品 电感耦合等离子体质谱法(ICP-MS)

2024

食品安全导刊
商业科技质量中心 北京肉类食品协会

食品安全导刊

影响因子:0.065
ISSN:1674-0270
年,卷(期):2024.(34)