食品工业2024,Vol.45Issue(1) :314-318.

GC-MS法分析两种新疆特色植物的油脂组成及挥发性成分

Analysis for Oil Composition and Volatile Compounds of Two Regional Characteristic Plants in Xinjiang by GC-MS

夏热帕提·吐孙 毛琼玲 熊燕
食品工业2024,Vol.45Issue(1) :314-318.

GC-MS法分析两种新疆特色植物的油脂组成及挥发性成分

Analysis for Oil Composition and Volatile Compounds of Two Regional Characteristic Plants in Xinjiang by GC-MS

夏热帕提·吐孙 1毛琼玲 2熊燕3
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作者信息

  • 1. 新疆工程学院化学与环境工程学院煤化工过程副产物高值转化协同创新中心(乌鲁木齐 830023)
  • 2. 新疆维吾尔自治区分析测试研究院(乌鲁木齐 830014)
  • 3. 新疆工程学院化学与环境工程学院煤化工过程副产物高值转化协同创新中心(乌鲁木齐 830023);重庆大学化学化工学院(重庆 401331)
  • 折叠

摘要

使用索氏提取器提取恰玛古籽的油脂,经过甲酯化,气相色谱-质谱法分析其油脂成分.恰玛古籽油脂主要含有顺-13-二十二碳一烯酸(51.64%)、反-9-十八碳一烯酸(18.55%)、反,反-9,12-十八碳二烯酸(10.79%)、顺-11-二十碳一烯酸(9.05%),不饱和脂肪酸占总脂肪酸含量的93.05%,饱和脂肪酸以十六碳酸为主.采用水蒸气蒸馏法对沙枣花中的挥发性成分进行提取,用GC-MS技术对其化学成分进行分离、鉴定,并用峰面积归一法确定各组分的相对含量,共鉴定出21种化合物.含量相对高的有甲基癸二酰氯(55.27%)、反式-肉桂酸乙酯(31.51%)、2,6-二叔丁基对甲苯酚(4.14%)、壬二酸二乙酯(2.01%)、反-9-十八碳一烯酸乙酯(1.69%)、愈创木醇(1.67%).

Abstract

The oil of Brassica rapa L.seed was extracted by the Soxhlet extraction method.After methyl esterification,the fatty acids in Brassica rapa L.seed oil were analyzed by CG-MS spectrometry.There were erucic acid(51.64%),oleic acid(18.55%),linoleic acid(10.79%),and arachidonic acid(9.05%)in Brassica rapa L.seed,unsaturated fatty acid was 93.05%,and palmitic acid was the main saturated fatty acid.The volatile oil from Elaeagnus angustifolia flower was extracted by steam distillation and analyzed by GC-MS.The peak area normalization method was used for quantification.Totally 21 compounds were identified and accounted for 96.29%of the total volatile oil,mostly including methyl 10-chloro-10-oxodecanoate(55.27%),ethyl trans cinnamate(31.51%),2,6-di-tert-butyl-4-methyl phenol(4.14%),Azelaic acid diethyl ester(2.01%),ethyl oleate(1.69%),and guaiacol(1.67%).

关键词

沙枣花/恰玛古籽/挥发性成分/水蒸气蒸馏/GC-MS

Key words

Elaeagnus angustifolia L./Brassica rapa L.seed/volatile components/steam distillation/GC-MS

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基金项目

国家自然科学基金(22161045)

新疆维吾尔自治区高校科研计划自然科学项目(XJEDU2017S060)

出版年

2024
食品工业
上海市食品工业研究所

食品工业

影响因子:0.47
ISSN:1004-471X
参考文献量20
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