首页|冷冻干燥法制备高强度果胶-二氧化硅复合气凝胶及其对花青素的递送

冷冻干燥法制备高强度果胶-二氧化硅复合气凝胶及其对花青素的递送

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二氧化硅气凝胶是一种新型的介孔纳米材料,应用广泛.在食品工业中,气凝胶主要作为包装、活性物质包埋递送及油凝胶的制备前体,主要通过其吸附性质达成.然而二氧化硅气凝胶结构主要由硅骨架构成,强度较低.因此,研究通过制备复合气凝胶来提高其性能.研究结果表明,适量添加果胶制备二氧化硅气凝胶(果胶含量10%)可使孔隙率最高达到95.3%,与二氧化硅复合改善了复合气凝胶的热稳定性.抗压结果表明,12.5%果胶添加量的气凝胶在100 g压力下形变量仅为80.6%,印证了果胶可以有效调节气凝胶的强度.吸附实验证明,添加果胶后对水蒸气的吸附程度增强,而对玉米油的吸附程度减弱,持油量增加.最后以花青素为模型,建立复合气凝胶对营养素的递送体系,复合气凝胶对花青素的控释有明显的效果,能够更好帮助营养素消化.该研究为复合气凝胶进一步在食品工业中的应用提供一定的理论依据.
Preparation of High Strength Pectin Silica Composite Aerogel by Freeze Drying and Its Delivery of Anthocyanins
Silica aerogel is a new kind of mesoporous nanomaterial,which is widely used.In the food industry,aerogel is mainly used as a precursor for packaging,embedding and delivering active substances,and preparing of oil gel,which is mainly achieved through its adsorption properties.However,the silica aerogel structure is mainly composed of silicon skeleton,and its strength is low.Therefore,this study aimed to improve its performance by preparing composite aerogels.The results showed that by adding an appropriate amount of pectin,the porosity of the silica aerogel(with 10%pectin)could reach up to 95.3%.The thermal stability of the composite aerogel was improved by compounding with SiO2.The compression test results showed that the deformation of aerogel with 12.5%pectin addition was only 80.6%under 100 g pressure,which confirmed that pectin could effectively regulate the strength of aerogel.Adsorption experiments have shown that the addition of pectin enhances the adsorption of water vapor,while the adsorption of corn oil weakens and the oil holding capacity increases.Finally,anthocyanins have been used as a model to establish the delivery system of compound aerogels for nutrients.Compound aerogels have significant effects on the controlled release of anthocyanins and can better help nutrients digestion.This study provides a theoretical basis for the further application of composite aerogels in the food industry.

silica aerogelpectinadsorption propertyanthocyanins

李艾潼、钟添宇、毛子鋆、韩旭杰、杨晨、汪建明

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天津科技大学食品科学与工程学院,天津 300457

二氧化硅气凝胶 果胶 吸附性 花青素

国家自然科学基金青年科学基金项目

32001626

2024

食品科技
北京市粮食科学研究所

食品科技

CSTPCD北大核心
影响因子:0.622
ISSN:1005-9989
年,卷(期):2024.49(8)