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SDE-GC-MS分析乌梅中挥发性成分

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为分析乌梅中挥发性成分的组成,采用同时蒸馏萃取(simultaneous distillation extraction,SDE)提取,气相色谱-质谱联用(gas chromatography-mass spectrometry,GC-MS)对乌梅中挥发性成分进行分析。从乌梅提取物中共鉴定出47种成分,主要包括酚类12种、酸类10种、酯类7种、杂环化合物6种、酮类4种、醛类4种和醇类2种等,其中糠醛(44.09%)、乙醇(12.71%)、苯甲醛(11.31%)、乙酸(7.33%)、十六酸(6.65%)、5-甲基糠醛(3.34%)、苯甲醇(2.04%)、乙酸乙酯(1.41%)和丁香酚(1.11%)。通过4次平行GC-MS分析,验证了定性定量结果的可靠性。
SDE-GC-MS Analysis of Volatile Compounds in Fructus Mume
The volatile compounds of Fructus Mume were extracted by simultaneous distillation-extraction(SDE) and analyzed by GC-MS.Forty-seven volatile compounds were identified including 12 phenols,10 acids,7 esters,6 herterocylic compounds,4 ketones,4 acetals and 2 alcohols.Among these compounds,furfural(44.09%),ethanol(12.71%),benzaldehyde(11.31%),acetic acid(7.33%),n-hexadecanoic acid(6.65%),5-methylfurfural(3.34%),benzyl alcohol(2.04%),ethyl acetate(1.41%) and eugenol(1.11%) were predominant.The qualitative and quantitative results obtained by the method were reliable,as validated by 4 parallel experiments.

Fructus Mumesimultaneous distillation extractionGC-MSanalysis

苗志伟、刘玉平、孙宝国

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北京工商大学食品学院 食品风味化学北京市重点实验室,北京100048

乌梅 同时蒸馏萃取 GC-MS 分析

北京市属高等学校人才强教计划项目

PHR20090504

2011

食品科学
北京食品科学研究院

食品科学

CSTPCDCSCD北大核心
影响因子:1.327
ISSN:1002-6630
年,卷(期):2011.32(24)
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