首页|基于GC-IMS技术的不同产地青钱柳茶挥发性成分表征及分析

基于GC-IMS技术的不同产地青钱柳茶挥发性成分表征及分析

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目的:研究不同产地青钱柳茶挥发性气味物质差异。方法:以湖南常德、湖南张家界、湖南邵阳、江西修水、贵州黔东南、湖北恩施的青钱柳茶为研究对象,采用气相色谱—离子迁移谱联用(GC-IMS)技术并结合偏最小二乘判别分析(PLS-DA),探讨不同产地青钱柳茶中特征差异挥发性物质及其相似度。结果:不同产地青钱柳茶共检测出120种挥发性有机物,包括部分物质的单体及其多聚体,分别为醛类34种、烯烃类21种、醇类19种、酮类16种、酯类10种、羧酸类8种、呋喃类5种、吡嗪类4种、醚类2种及苯系物1种。其中γ-松油烯、苯乙烯、4-甲基-1-戊醇、正辛醛为主要特征差异挥发性物质。结论:不同产地间青钱柳茶挥发性有机物质均存在一定差异(P<0。05),GC-IMS技术可有效实现青钱柳茶的产地鉴别和质量控制。
Characterization and analysis of the volatile components of Cyclocarya paliurus tea from different origins based on GC-IMS technology
Objective:To investigate the differences in volatile odor substances of Cyclocarya paliurus tea from different origins.Methods:Taking Cyclocarya paliurus tea from Changde,Zhangjiajie,Shaoyang in Hunan,Xiushui in Jiangxi,Qiandongnan in Guizhou,and Enshi in Hubei as the research subjects,the gas chromatography-ion mobility spectrometry(GC-IMS)coupled with partial least squares discriminant analysis(PLS-DA)was used to investigate the characteristics of different volatiles and their similarities in green strychnine teas from different origins.Results:A total of 120 VOCs,including monomers of some substances and their polymers,were detected in Cyclocarya paliurus tea from different origins,which were 34 aldehydes,21 olefins,19 alcohols,16 ketones,10 esters,8 carboxylic acids,5 furans,4 pyrazines,2 ethers,and 1 benzene species,respectively.Among them,γ-pinene,styrene,4-methyl-1-pentanol,and n-octanal were the main characteristic difference volatiles.Conclusion:There were some differences in the volatile organic compounds of Cyclocarya paliurus tea among different origins(P<0.05).It is possible to distinguish between different origins of cymbopogon tea based on the characteristic volatile substances.GC-IMS technology can effectively realize the origin identification and quality control of GC tea.

Cyclocarya paliurus teavolatile substancesgas chromatography-ion mobility spectrometry(GC-IMS)partial least squares discriminant analysis(PLS-DA)dynamic principal component analysis

罗洁、邹雅倩、田星

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湖南中医药大学药学院,湖南长沙 410208

湖南省中医药民族医药国际联合实验室,湖南长沙 410208

青钱柳茶 挥发性物质 气相色谱—离子迁移谱 偏最小二乘判别 主成成分析

湖南中医药大学本科生科研创新基金湖南中医药大学本科生科研创新基金湖南中医药大学学科建设"揭榜挂帅"项目

2023BKS1052023BKS19022JBZ053

2024

食品与机械
长沙理工大学

食品与机械

CSTPCD北大核心
影响因子:0.89
ISSN:1003-5788
年,卷(期):2024.40(5)