食品与机械2024,Vol.40Issue(9) :44-49.DOI:10.13652/j.spjx.1003.5788.2024.60081

油凝胶改善二氧化硅颗粒薄荷醇的吸附性能

Study on improving menthol adsorption performance of silica particles by olege

魏玉磊 郭鹏 高云 刘群 张豪洋 邹立强
食品与机械2024,Vol.40Issue(9) :44-49.DOI:10.13652/j.spjx.1003.5788.2024.60081

油凝胶改善二氧化硅颗粒薄荷醇的吸附性能

Study on improving menthol adsorption performance of silica particles by olege

魏玉磊 1郭鹏 1高云 1刘群 1张豪洋 1邹立强2
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作者信息

  • 1. 山东中烟工业有限责任公司,山东 济南 250100
  • 2. 南昌大学食品科学与资源挖掘全国重点实验室,江西 南昌 330047
  • 折叠

摘要

[目的]改善二氧化硅的薄荷醇吸附性能.[方法]采用二氧化硅吸附熔融薄荷醇油凝胶制备附香颗粒,探究棕榈油的添加比例对油凝胶硬度、保油率、热力学特性的影响.对比附香颗粒的微观形态、流动性能及其负载薄荷醇的包封率、贮藏稳定性和释放特性,并评价油凝胶对二氧化硅颗粒的吸附性能改善作用.[结果]当棕榈油添加量为50%,80%时,油凝胶保油率均在90%以上,油凝胶的硬度和熔融峰值温度随棕榈油比例的提高而增大.微观结果显示,附香颗粒表面有油凝胶附着,薄荷醇包封率由 73.43%提高至 82.05%和 91.19%,贮藏终点包封率由 30.77%提高至69.83%和80.28%,且有效改善了薄荷醇的缓释性能.[结论]油凝胶能有效改善二氧化硅颗粒的薄荷醇吸附性能.

Abstract

[Objective]To improve the menthol adsorption properties of silica.[Methods]Fragrance-absorbing particles were prepared using silica adsorption-melted menthol oleogel.The impact of palm oil addition ratio on the oleogel hardness,oil binding capacity,and thermodynamic properties was investigated.Comparative particles microstructure,flow properties,and the loaded menthol encapsulation efficiency,storage stabilityand release characteristics to assess the enhancement of silica particle adsorption properties by the oleogel.[Results]When palm oil addition ratio were 50%and 80%,the oil binding capacity of oleogels were over 90%,and the hardness and peak melting temperature of the gels increased with the palm oil ratio.Microscopic observations revealed the adsorption of oleogels on the surface of silica particles.Encapsulation efficiency of menthol increased from 73.43%to 82.05%and 91.19%,while storage endpoint encapsulation efficiency rose from 30.77%to 69.83%and 80.28%.Concurrently,menthol sustained-release properties were enhanced.[Conclusion]Oleogel effectively improves the adsorption properties of silica particles for menthol.

关键词

油凝胶/薄荷醇/二氧化硅颗粒/包封率/缓释

Key words

oleogel/menthol/silica particles/encapsulation efficiency/sustained-release

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基金项目

国家自然科学基金项目(32160563)

校企合作项目(2023370000340521)

校企合作项目(2024370000340145)

出版年

2024
食品与机械
长沙理工大学

食品与机械

CSTPCD北大核心
影响因子:0.89
ISSN:1003-5788
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