实验科学与技术2025,Vol.23Issue(1) :34-41.DOI:10.12179/1672-4550.20230416

淀粉基碳点材料的合成及用于潜指纹提取实验设计

Comprehensive Research of Synthesis and Fingerprint Detection of Starch-Based Carbon Dots Fluorescent Materials

李俊玲 罗蓉 苏群 雷雨 房川琳
实验科学与技术2025,Vol.23Issue(1) :34-41.DOI:10.12179/1672-4550.20230416

淀粉基碳点材料的合成及用于潜指纹提取实验设计

Comprehensive Research of Synthesis and Fingerprint Detection of Starch-Based Carbon Dots Fluorescent Materials

李俊玲 1罗蓉 2苏群 2雷雨 2房川琳1
扫码查看

作者信息

  • 1. 四川大学化学实验教学中心,成都 610207
  • 2. 四川大学化学学院,成都 610065
  • 折叠

摘要

碳量子点(CDs)具有特殊的光学性质和良好的生物相容性,是近几年科研领域一种热门的荧光纳米材料.该项目在科教融汇教学理念的指导下,将科研热点与本科实验教学相结合,探究了反应物配比、反应方式、反应时长、产物浓度、溶液pH等多项制备条件对碳点材料性能的影响.研究结果表明:采用尿素与柠檬酸为原材料,控制两者的配比为1∶3,微波高火反应 2.5~4 min或马弗炉 200℃反应 1.0 h,均可获得荧光性能良好的碳点材料.在综合创新实验课堂中,学生在合成的碳点材料中引入淀粉基底,所得的淀粉基碳点荧光材料可应用于多场景的指纹提取.实验培养学生的创新与发散思维,增强学生在社会安全领域的参与感与社会责任感.

Abstract

In recent years,carbon dots(CDs)with special optical properties and excellent biocompatibility,have become a popular fluorescent nanomaterial in scientific research.Under the guidance of science education integration,the project combines scientific hot spot with undergraduate experimental teaching.Series of experiments are designed to investigate the effects of experimental conditions,such as reactant ratio,reaction mode,reaction duration,product concentration and pH value on the properties of materials.The results show that CDs with good fluorescence properties can be obtained by controlling the ratio of urea and citric acid at 1∶3.The reaction mode is microwave high fire for 2.5~4 min or muffle furnace reaction at 200℃for 1.0 h.In the comprehen-sive innovation experiment class,the starch-based CDs fluorescent powder can be obtained,by introducing starch substrate into CDs,which is adaptable for the fingerprint detection in multiple scenes.As a result,the scientific innovation which is divergent thinking of students will be cultivated and enhanced,as well as the sense of participation and social responsibility in the field of social security.

关键词

碳量子点/荧光材料/指纹检测

Key words

carbon dots/flourescent material/fingerprint detection

引用本文复制引用

出版年

2025
实验科学与技术
四川省高教学会,电子科技大学

实验科学与技术

影响因子:0.762
ISSN:1672-4550
段落导航相关论文