首页|EAF+VAR生产15-5PH不锈钢点状缺陷成因及改进

EAF+VAR生产15-5PH不锈钢点状缺陷成因及改进

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采用冶炼成本较低的EAF→VOD→LF+VD→浇注6 t电极棒→真空自耗重熔(VAR)的新工艺流程代替传统双真空冶炼工艺生产15-5PH不锈钢,使用扫描电镜、ASPEX等对其探伤点状缺陷进行检测,并分析其产生原因.结果表明,自耗电极中已存在铝酸钙及镁铝尖晶石非金属夹杂物,真空自耗重熔过程的不稳定,将锭冠和非金属漂浮物卷入熔池残留在自耗锭中,导致锻造成材后产生点状缺陷.通过工艺优化改进,VOD还原渣料由铝粒9 kg/t调整为硅铁8 kg/t、铝粒5 kg/t复合脱氧,精炼渣系成分由(质量分数)CaO为50%~55%、SiO2为10%~15%、Al2O3为20%~25%调整为CaO为45%~50%、SiO2为5%~10%、Al2O3为33%~38%,真空自耗重熔熔速由4.2 kg/min提高至6 kg/min、熔滴时间由0.23 s提高至0.27 s,自耗电极洁净度得到较大的提升,自耗重熔过程熔速控制稳定,熔池液面非金属漂浮物得以去除,成品材高低倍检验均满足标准要求,探伤合格率提高至98%以上.
Causes and Improvement of Point Defects in 15-5PH Stainless Steel Producted by EAF+VAR
The new process of EAF→VOD→LF+VD→ pouring 6 t electrode rod → vacuum consumable remelting(VAR)with lower smelting cost was adopted to produce 15-5PH stainless steel instead of the traditional VIM+VAR process,the causes of point defects were analyzed by scanning electron microscopy and ASPEX detection methods.The results show that calcium aluminate and aluminum spinite exist in the self-consuming electrode,the instability of vacuum consumable remelting process will draw the ingot crown and non-metallic float into the melting pool and remain in the consumable in-got,resulting in point defects after forging.Through process optimization and improvement,the VOD reduction slag is ad-justed from 9 kg/t aluminum to 8 kg/t ferrosilicon and 5 kg/t aluminum,the composition of refining slag is adjusted from(mass fraction)CaO 50%-55%,SiO2 10%-15%,Al2O3 20%-25%to CaO 45%-50%,SiO2 5%-10%,Al2O3 33%-38%,vacuum consumable remelting speed is increased from 4.2 kg/min to 6 kg/min,and the melting drop time is increased from 0.23 s to 0.27 s,the cleanliness of consumable electrode has been greatly improved,the melting speed has been con-trolled steadily,the non-metal floating matter on the liquid surface of the molten pool has been removed,low and high mag-nification inspection of the finished material have met the standard requirements,and the inspection pass rate has been in-creased to more than 98%.

15-5PH Stainless SteelPoint DefectsRefining Slag SystemVARDroplet Time

章东海、潘明旭、李旭、许勇、熊皓

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大冶特殊钢有限公司锻造事业部,黄石 435001

大冶特殊钢有限公司,黄石 435001

15-5PH不锈钢 点状缺陷 精炼渣系 真空自耗重熔 熔滴时间

2024

特殊钢
中国金属学会特殊钢分会 大冶特殊钢股份有限公司

特殊钢

影响因子:0.345
ISSN:1003-8620
年,卷(期):2024.45(4)
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