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藏药白亮独活的质量标准研究

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目的 为了更好地规范和控制藏药白亮独活的质量,对其进行质量标准研究,为白亮独活的质量控制提供科学的依据.方法 参照《中华人民共和国药典》2020年版中规定的相关方法,对白亮独活药材的性状、显微特征以及各检查项进行检测;采用薄层色谱法,以硅胶G为薄层板,石油醚(60~90)-乙酸乙酯(3:1)为展开剂,欧前胡素为对照品,建立其薄层鉴别方法.结果 准确描述了藏药白亮独活的显微鉴别特征和薄层鉴别特征.其水分为9.9%~11.0%,总灰分为5.4%~9.1%,酸不溶性灰分为0.79%~4.98%,水溶性浸出物的含量为30.71%~38.83%.结论 该研究首次全面考察了西藏地区白亮独活药材的各项质量指标,能有效评价其质量.
Study on the Quality Standards of Tibetan Medicine Bailiang Duhuo
Objective In order to better standardize and control the quality of Tibetan medicine Bailiang Duhuo,the quality standards were studied so as to provide a scientific basis for its quality control.Methods Referring to the rel-evant methods specified in the 2020 edition of the Pharmacopoeia of the people's Republic of China,the characters,microscopic characteristics and inspection items of Bailiang Duhuo medicinal materials were detected.The thin-layer chromatography(TLC)method was used to establish a thin-layer identification method with silica gel G as the thin-layer plate,petroleum ether(60-90)-ethyl acetate(3:1)as the developing solvent,and imperatorin as the reference substance.Results The microscopic identification characteristics and thin-layer identification characteristics of Ti-betan medicine Bailiang Duhuo were described accurately.Its moisture content is 9.9%-11.0%,the total ash is 5.4%-9.1%,the acid-insoluble ash is 0.79%-4.98%,and the content of water-soluble extract is 30.71%-38.83%.Conclusion This study was the first to comprehensively investigate the quality indexes of Bailiang Duhuo medicinal materials in Xizang,and its quality could be effectively evaluated.

Bailiang DuhuoQuality standardTLC identificationMicroscopic identification

岗格措、才让南加、占堆

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西藏藏医药大学,拉萨 850000

白亮独活 质量标准 薄层鉴别 显微鉴别

西藏藏医药大学中药学博士点培育项目

BSTD-202302

2024

西藏科技
西藏科技信息研究所

西藏科技

影响因子:0.202
ISSN:1004-3403
年,卷(期):2024.46(5)
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