首页|山东省某市市售鸡蛋和鸡肉中硝基咪唑类药物残留检测分析

山东省某市市售鸡蛋和鸡肉中硝基咪唑类药物残留检测分析

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目的 了解山东省某市市售鸡蛋和鸡肉中硝基咪唑类药物的残留情况.方法 2021年6-8月,从山东省某市农贸市场和超市等场所采集鸡蛋样品10份、鸡肉样品30份,采用超高效液相色谱-串联质谱法(UPLC-MS/MS)测定样品中5种硝基咪唑类药物的残留量.结果 在40份样品中9份检出硝基咪唑类药物残留,检出率为22.50%(9/40).在2份鸡蛋样品中检出药物残留、检出率为20%(2/10),其中1份检出甲硝唑、含量为124 μg/kg,另外1份检出地美硝唑、含量为214 μg/kg.在30份鸡肉样品中,1份检出甲硝唑、含量为2.65 μg/kg,7份检出罗硝唑、含量为0.26~3.59 μg/kg.结论 山东省某市市售鸡蛋和鸡肉样品中存在硝基咪唑类药物残留情况.
Monitoring results analysis of nitroimidazole drug residues in eggs and chicken from markets
Objective To understand the nitroimidazole drug residues in eggs and chicken from markets.Methods The residues of 5 nitroimidazole drugs in a total of 10 egg samples and 30 chicken samples,collected from farmers'markets and supermarkets in a city of Shandong Province between June and August 2021.Samples were determined by using ultra-high performance liquid chromatography-tandem mass spectrometry(UPLC-MS/MS).Results Drug residue was detected in 9 of 40 samples,the total detection rate was 22.50%.In terms of classification,drug residues were detected in 2 egg sam-ples,the detection rate was 20%.Metronidazole(124 μg/kg)was detected in 1 sample,the content of dimecnidazole was 214 μg/kg in the other one.Metronidazole(2.65 μg/kg)was detected in 1 sample of 30 chicken samples.Ronidazole was detected in 7 samples with the content ranging from 0.26 to 3.59 μg/kg.Conclusion The presence of nitroimidazole residues was detected in eggs and chicken samples sold within a city located in Shandong province.

EggChickenNitroimidazoleDrug residueUPLC-MS/MS

张远、葛文娜、霍海波、郑凤家、姜大峰、李华锋

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山东医学高等专科学校医学检验系,山东济南 250002

曲阜市疾病预防控制中心

山东医学高等专科学校药学系

山东省疾病预防控制中心卫生检验检测所

山东医学高等专科学校组织人事处

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鸡蛋 鸡肉 硝基咪唑 药物残留 超高效液相色谱-串联质谱法

山东省医药卫生科技发展计划山东省医药卫生科技发展计划

202112060707202112061045

2024

预防医学论坛
中华预防医学会

预防医学论坛

影响因子:0.645
ISSN:1672-9153
年,卷(期):2024.30(2)
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