首页|应用Minitab软件进行磁铁矿中二氧化硅质量控制分析及评价

应用Minitab软件进行磁铁矿中二氧化硅质量控制分析及评价

扫码查看
实验室内部质量控制多以标准物质为分析对象,测量值与标准物质认定值的绝对差值和临界值比较,采用Excel或Wps软件可实现结果的分析与评价,评价手段对评价者的能力要求不高,但不适用于量大的临界值计算.Minitab软件是现代质量管理中的重要工具,功能强大,可快速实现数据的均值、正态、标准化四分位距、异常值、质控图、尧敦图等统计.实验利用Minitab软件对磁铁矿中二氧化硅的对样质量监控数据进行分析,采用3种临界值公式进行评价.结果表明:采用中间精密度临界值的评价结果95%满意,临界值约为其他方法的35%~83%,说明采用中间精密度临界值评价能达到严格质控目的.统计A样、B样的Z比分数,只有B样的第37组结果可疑.进一步统计对样实验室间Z比分数(ZB)和实验室内Z比分数(Zw),数据表明第19组数据的ZB值为-2.19,第34组数据的Zw值为2.59,这两组数据均可疑.通过Minitab软件能实现对质控结果的快速统计,有效发现可疑数据,进一步纠正人员不规范操作,具有很强的实践意义.
Application of Minitab software for quality control analysis and evaluation of silicon dioxide in magnetite
The reference materials are usually used as analytical samples for internal quality control in labo-ratories.The absolute difference value between the measured value and the certified value of reference ma-terial is compared with the critical value.The analysis and evaluation of results can be realized using Excel or Wps software,which doesn't require high ability for the evaluators.However,it is not suitable for the critical value calculation with a large number of tests.Minitab software is an important tool in modern qual-ity management with powerful functions,which can quickly realize the data statistics such as mean,normal-ity,norm interquartile range(IQR),outlier,quality control chart and Youden plot.In this study,Minitab software was used to analyze the double samples quality control data of silicon dioxide in magnetite,and three kinds of critical value formulas were used for evaluation.The results showed that the evaluation re-sults of intermediate precision critical value were 95%satisfactory,and the critical value was about 35%-83%of other methods,indicating that the evaluation of intermediate precision critical value could achieve the purpose of strict quality control.According to the Z-scores of sample A and sample B in statistic,only the results of 37th group were suspicious.The inter-laboratory Z-score(ZB)and intra-laboratory Z-score(Zw)were further analyzed,and the results showed that the values of two groups were suspicious:the ZB value of the 19th group data was-2.19,and the Zw value of the 34th group data was 2.59.Rapid statistics of quality control results could be achieved by Minitab software to effectively find out the suspicious data and further correct the non-standard operation of personnels.Therefore,it had a strong practical signifi-cance.

quality controlMinitab softwaresilicon dioxidemagnetitecritical valueintermediate preci-sionevaluation

邓军华、胡忠新、杨洁、亢德华

展开 >

海洋装备用金属材料及其应用国家重点实验室,辽宁鞍山 114009

鞍钢集团钢铁研究院,辽宁鞍山 114009

质量控制 Minitab软件 二氧化硅 磁铁矿 临界值 中间精密度 评价

2024

冶金分析
中国钢研科技集团有限公司(钢铁研究总院) 中国金属学会

冶金分析

CSTPCD北大核心
影响因子:1.124
ISSN:1000-7571
年,卷(期):2024.44(7)