首页|Additive-free synthesis of β-keto phosphorodithioates via geminal hydro-phosphorodithiolation of sulfoxonium ylides with P4S10 and alcohols
Additive-free synthesis of β-keto phosphorodithioates via geminal hydro-phosphorodithiolation of sulfoxonium ylides with P4S10 and alcohols
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A simple and additive-free protocol has been developed for the preparation of β-keto phospho-rodithioates through the three-component reaction of easily available sulfoxonium ylides,P4S10,and alco-hols.The present geminal hydro-phosphorodithiolation reaction was performed at room temperature to construct a series of β-keto phosphorodithioates in the absence of any metal reagents,bases,or additives.
Jindong Hao、Yufen Lv、Shuyue Tian、Chao Ma、Wenxiu Cui、Huilan Yue、Wei Wei、Dong Yi
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Key Laboratory of Catalytic Conversion and Clean Energy in Universities of Shandong Province,School of Chemistry and Chemical Engineering,Qufu Normal University,Qufu 273165,China
Qinghai Provincial Key Laboratory of Tibetan Medicine Research and CAS Key Laboratory of Tibetan Medicine Research,Northwest Institute of Plateau Biology,Xining 810008,China
Green Pharmaceutical Technology Key Laboratory of Luzhou City,School of Pharmacy,Southwest Medical University,Luzhou 646000,China
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