中国粮油学报2024,Vol.39Issue(1) :182-188.DOI:10.20048/j.cnki.issn.1003-0174.000177

玉兰叶多酚物质提取及特性研究

Extraction and Characteristics of Magnolia Polyphenols

张顺 惠哲哲 王宏亮 杨瑞 梁犇 杨骏鹏 邱莹 宋凤敏 刘存芳 高艳红 史娟
中国粮油学报2024,Vol.39Issue(1) :182-188.DOI:10.20048/j.cnki.issn.1003-0174.000177

玉兰叶多酚物质提取及特性研究

Extraction and Characteristics of Magnolia Polyphenols

张顺 1惠哲哲 1王宏亮 1杨瑞 1梁犇 1杨骏鹏 1邱莹 1宋凤敏 1刘存芳 1高艳红 1史娟1
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作者信息

  • 1. 陕西省催化重点实验室;陕西理工大学化学与环境科学学院,汉中 723001
  • 折叠

摘要

利用超声波提取法,以乙醇为溶剂对玉兰叶多酚进行提取.选择乙醇体积分数、料液比、超声温度和超声时间作为影响因素.在单因素实验的基础上,通过正交实验对玉兰多酚的提取条件进行优化,经紫外光照、添加剂、氧化剂、还原剂、金属离子和热处理后,研究了玉兰叶多酚的抗氧化稳定性.同时研究玉兰叶多酚对油脂基质的抗氧化性质.结果表明:以乙醇为提取溶剂时,玉兰多酚的最佳提取工艺为乙醇体积分数为80%,料液比1∶16,超声温度80℃,超声时间40 min.玉兰叶多酚对自由基清除作用试验表明,多酚对DPPH自由基和羟自由基均具有清除作用,对DPPH自由基清除能力较好.多酚提取物可以有效地延缓植物油及动物油的氧化,抗氧化能力随着玉兰叶多酚提取物添加量的增加而增强.

Abstract

The extraction of polyphenols from Magnolia grandiflora was conducted by ultrasonic extraction with ethanol as solvent.The ethanol concentration,solid-liquid ratio,ultrasonic temperature and ultrasonic time were se-lected as influencing factors.On the basis of single factor experiment,the extraction conditions of polyphenol were studied by orthogonal test.The antioxidant stability of polyphenols was studied by UV irradiation,additives,oxi-dants,reducing agents,metal ions and heat treatment.At the same time,the antioxidant properties of polyphenols from leaves of Magnolia on oil matrix were studied.The results indicated that the optimum extraction conditions were as follows:ethanol concentration of 80%,material ratio of 1:16,ultrasonic temperature of 80℃,ultrasonic time of 40 min.The results indicated that polyphenol had a scavenging effect on DPPH free radical and hydroxyl radical and had better scavenging ability on DPPH free radicals.The results indicated that the polyphenols from leaves of Magno-lia could effectively delay the oxidation of vegetable oil and animal oil,and the antioxidant capacity increased with the increase of polyphenols from leaves of Magnolia.

关键词

玉兰叶多酚/超声波提取/抗氧化

Key words

magnolia leaf polyphenols/ultrasonic extraction/antioxidant

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基金项目

陕西理工大学秦巴生物资源与生态环境省部共建国家重点实验室项目(SXJ-2106)

陕西省科技厅社会发展科技攻关项目(2021SF-382)

出版年

2024
中国粮油学报
中国粮油学会

中国粮油学报

CSTPCD北大核心
影响因子:1.056
ISSN:1003-0174
参考文献量18
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