中国粮油学报2024,Vol.39Issue(7) :43-51.DOI:10.20048/j.cnki.issn.1003-0174.000837

提取方法对米糠纤维素理化性质的影响

Effects of Extraction Methods on Physicochemical Properties of Rice Bran Cellulose

郭逍 罗诗烨 林炎鑫 林亲录 丁玉琴 李晶 龚艳玲 郑晓春
中国粮油学报2024,Vol.39Issue(7) :43-51.DOI:10.20048/j.cnki.issn.1003-0174.000837

提取方法对米糠纤维素理化性质的影响

Effects of Extraction Methods on Physicochemical Properties of Rice Bran Cellulose

郭逍 1罗诗烨 1林炎鑫 1林亲录 1丁玉琴 1李晶 2龚艳玲 2郑晓春2
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作者信息

  • 1. 中南林业科技大学食品科学与工程学院,长沙 410000
  • 2. 美的电热电器制造有限公司,佛山 528300
  • 折叠

摘要

以脱脂米糠为原料提取米糠不溶性膳食纤维(IDF),采用氢氧化钠-亚氯酸钠法、超声辅助氢氧化钠-亚氯酸钠法、氢氧化钠-过氧化氢法、超声辅助氢氧化钠-过氧化氢法等四种方法提取米糠纤维素,并比较4种提取方法对米糠纤维素结构特性和功能特性的影响.结果表明,超声辅助氢氧化钠-亚氯酸钠法提取纤维素具有最高纯度(88.69%)和结晶度(59.30%),且有较好热稳定性、持水性、持油性和葡萄糖吸附能力.与氢氧化钠-亚氯酸钠法相比,氢氧化钠-过氧化氢法提取的纤维素的平均粒径小,持水性和持油能力弱,而胆酸盐吸附能力和淀粉酶抑制活性更强.FT-IR图谱表明氢氧化钠-过氧化氢法提取的纤维素中含有一定量的木质素和半纤维素.SEM分析表明氢氧化钠-亚氯酸钠法提取的米糠纤维素表面更加光滑,超声辅助处理可以显著提高了纤维素的纯度以及持水性和持油性,但对纤维素的平均粒径、热稳定性无显著影响.

Abstract

The insoluble dietary fiber(IDF)was extracted from rice bran by using degreased rice bran as raw material.Four methods were used to extract rice bran cellulose,including sodium hydroxide-sodium chlorite,ultra-sonic-assisted sodium hydroxide-sodium chlorite,sodium hydroxide-hydrogen peroxide,ultrasonic-assisted so-dium hydroxide-hydrogen peroxide.The effects of four extraction methods on the structural and functional character-istics of rice bran cellulose were compared.The results indicated that ultrasonic assisted extraction of cellulose with sodium hydroxide and sodium chlorite had the highest purity(88.69%)and crystallinity(59.30%),and had better thermal stability,water retention,oil retention and glucose adsorption capacity.Compared with the sodium hydroxide-sodium chlorite method,the average particle size of cellulose extracted by the sodium hydroxide-hydro-gen peroxide method was smaller,the water holding capacity and oil holding capacity were weaker,and the cholate adsorption capacity and amylase inhibiting activity were stronger.FT-IR spectra revealed that the cellulose extracted by sodium hydroxide and hydrogen peroxide method contained a certain amount of lignin and hemicellulose.SEM analysis indicated that the surface of rice bran cellulose extracted by sodium hydroxide-sodium chlorite was smoot-her.Ultrasonic assisted treatment significantly improved the purity,water and oil retention of cellulose,but did not have significant effects on the average particle size and thermal stability of cellulose.

关键词

米糠/纤维素/碱法提取/超声处理/结构性质/吸附能力

Key words

rice bran/cellulose/alkali extraction/ultrasonic treatment/structural property/adsorption capacity

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基金项目

湖南省科技创新计划项目(2023ZJ1070)

中央引导地方科技资金项目(2023ZYC008)

湖南省"洞庭香米"优势特色产业集群项目(湘农联[2022]79号)

出版年

2024
中国粮油学报
中国粮油学会

中国粮油学报

CSTPCD北大核心
影响因子:1.056
ISSN:1003-0174
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