首页|一种基于近红外光谱的饲用鸭油特征脂肪酸含量快速测定方法

一种基于近红外光谱的饲用鸭油特征脂肪酸含量快速测定方法

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为对饲用鸭油特征脂肪酸进行快速预测,本研究建立了基于近红外光谱预测饲用鸭油棕榈酸、棕榈-烯酸、硬脂酸、油酸、亚油酸、亚麻酸6种脂肪酸含量的方法。用国标法测试鸭油样品脂肪酸组成,并采集近红外光谱。使用标准正态变换(SNV)等方法对光谱信息进行预处理,筛选出最优光谱预处理方法。采用改进型偏最小二乘法(mPLS),以1-VR(交互验证决定系数)和SECV值(交互验证标准差)为评价指标,建立预测模型。结果表明:1)用验证集样品对模型进行外部独立验证,验证结果的SEP(验证标准差)、SEC(校正标准差)符合AACC 39-00规定的"SEP/SEC≤1。2"原则。2)油酸模型、棕榈酸模型、棕榈一烯酸模型、硬脂酸模型、亚油酸模型和亚麻酸模型的R2(外部验证决定系数)分别为0。918、0。889、0。916、0。869、0。979和0。927,表明所建立近红外预测模型可对饲用鸭油的6种脂肪酸含量进行有效预测。本研究建立的饲用鸭油特征脂肪酸快速检测方法能够满足一定程度的快检需求,为评价饲用鸭油质量提供快速、便捷的技术方法和理论参考。
A method for quickly predicting fatty acid content of feed duck oil based on near-infrared spectroscopy
To rapidly predict characteristic duck oil fatty acid content,this study established a method to predict the content of six fatty acids including palmitic acid,palmitoleic acid,stearic acid,oleic acid,linoleic acid,and linolenic acid based on near-infrared spectroscopy.Gas chromatographic method was used to test the fatty acid composition of samples and collect near-infrared spectra.Standard Normal Variate Transformation(SNV)and other methods were used to preprocess the spectral information,and the optimal spectral preprocessing method was selected.The improved partial least square method(mPLS)was used to establish an optimal near-infrared prediction model with 1-VR(Determination coefficient of SECV)and SECV values(Standard error of cross validation).The results showed that:1)This model was independently verified with the validation set samples,The SEP(Standard error of prediction)and SEC(Standard error of calibration)of the verification results were in accordance with the"SEP/SEC≤1.2"principle stipulated in AACC 39-00.2)The R2 of the palmitic acid,palmitoleic acid,stearic acid,oleic acid,linoleic acid,and linolenic was 0.889、0.916、0.869、0.918、0.979 and 0.927,indicating that the established near-infrared prediction model can effectively predict the content of six fatty acids in duck oil.The rapid detection method for characteristic fatty acids n feed duck oil established in this study could meet a certain degree of rapid detection needs,providing a fast and convenient technical method and theoretical reference for evaluating the quality of feed duck oil.

feeding duck oilfatty acidnear-infraredrapid detection technology

包郁明、李亮、范志影、谷旭、赵维香、朱超、李春红、马莹

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中国农业科学院饲料研究所,北京 100081

福斯华(北京)科贸有限公司,北京 100081

中国农业科学院农产品加工研究所,北京 100193

饲用鸭油 脂肪酸 近红外 快检技术

2025

中国农业大学学报
中国农业大学

中国农业大学学报

北大核心
影响因子:0.971
ISSN:1009-508X
年,卷(期):2025.30(1)