中国乳业2024,Issue(11) :144-148,156.DOI:10.12377/1671-4393.24.11.23

基于中红外光谱的牛乳中A2β-酪蛋白检测方法研究

Detection of A2β-casein in Milk Based on Mid-infrared Spectroscopy

杨戬 刘伯扬 王丹慧 高永亮 赵三军 赵凯 李慧 仪虹伯
中国乳业2024,Issue(11) :144-148,156.DOI:10.12377/1671-4393.24.11.23

基于中红外光谱的牛乳中A2β-酪蛋白检测方法研究

Detection of A2β-casein in Milk Based on Mid-infrared Spectroscopy

杨戬 1刘伯扬 1王丹慧 1高永亮 1赵三军 1赵凯 1李慧 1仪虹伯1
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作者信息

  • 1. 内蒙古蒙牛乳业(集团)股份有限公司,内蒙古呼和浩特 011517
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摘要

[目的]研究基于中红外光谱的牛乳中A2β-酪蛋白检测方法.[方法]进行光谱采集,利用多元散射校正及标准正态化预处理提高光谱信噪比,在竞争自适应重加权算法筛选得到特征变量基础上,建立基于偏最小二乘的定量分析模型.[结果]预处理及变量筛选后,训练、预测误差分别达到0.061 g/100 g、0.068 g/100 g,R分别达到0.893、0.875.[结论]中红外光谱方法可用于牛乳中A2β-酪蛋白快速检测,光谱预处理、特征变量提取方法显著提高建模精度,可为牛乳中其他成分的光谱检测方法准确性提供参考.

Abstract

[Objective]A method for the detection of A2β-casein in milk based on mid-infrared spectroscopy is investigated.[Method]The MIR spectrum of milk samples were measured and preprocessed with multiple scattering correction and standard normalization to improve the signal-to-noise ratio.Then,the characteristic variables were selected by the competitive adaptive reweighting algorithm.The quantitative analysis model based on partial least squares was established.[Result]After pre-processing and variable screening,the training and prediction errors reached 0.061 g/100 g and 0.068 g/100 g,respectively,and the R reached 0.893 and 0.875,respectively.[Conclusion]The mid-infrared spectroscopy method can be used for the rapid detection of A 2β-casein in milk.The spectral pre-processing and characteristic variables extraction methods can significantly improve the modelling accuracy.It also provided a good basis for the spectral detection methods for other ingredients in milk.

关键词

中红外光谱/A2β-酪蛋白/预处理/竞争自适应重加权采样

Key words

mid-infrared spectroscopy/A2β-casein/pre-processing/competitive adaptive reweighting sampling

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出版年

2024
中国乳业
中国奶业协会 中国农业科学院信息研究所

中国乳业

影响因子:0.152
ISSN:1671-4393
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