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白背叶黄酮类成分的研究

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采用反复聚酰胺柱以及高效液相色谱等方法分离白背叶黄酮提取物中的化学成分,运用化学和有机波谱分析方法确定化合物结构.从白背叶乙酸乙酯提取物中分离得到5个黄酮类化合物,经鉴定分别为(1)葫芦芭苷Ⅱ,(2)异夏佛托苷,(3)夏佛托苷,(4)大波斯菊苷和(5)洋芹素.其中,异夏佛托苷和夏佛托苷为首次从该植物及该属植物中分离得到.
Study on flavonoids constituent in Mallotus apelta
Compounds from Mallotus apelta were isolated by a combination of polyamide columnar chromatography and HPLC method.The compounds' structure were identified by chemical and spectral Methods .Five kinds of flavonoids were isolated from Mall-otus apelta ethyl acetate extracts by HPLC techniques and their structures were determined through spectral analysis(1H,13C-NMR and MS)and comparison with the literature data.Their structures were identified as(1)vicentⅡ,(2)isoschaftoside,(3)schaftoside,(4)apigenin-7-O-β-D-glucopyranoside and(5)apigenin.In addtion, isoschaftoside and schaftoside is the first time obtained from Mallotus apelta.

Mallotus apeltachemical constituentflavonoidchromatographic separationspectrum analysis

张婕、王立慈、张斌

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山东大学第二医院 药学部,山东 济南 250033

白背叶 化学成分 黄酮 色谱分离 波普解析

2017

中国生化药物杂志
南京生物化学制药研究所,全国生化制药情报中心站,中国生化制药工业协会,中国药品生物制品检定所

中国生化药物杂志

ISSN:1005-1678
年,卷(期):2017.(7)
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