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不同贮藏时间即食燕窝特征风味成分分析

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为探究不同贮藏时间即食燕窝的风味特征,采用气相色谱-离子迁移谱(GC-IMS)对5个贮藏时间市售即食燕窝的挥发性有机物进行差异分析.结果表明,不同贮藏时间即食燕窝的挥发性成分存在显著差异(P<0.05),共鉴定出44个挥发性有机物(包含单聚体和二聚体),主要为醛和酯类.主成分分析(PCA)和偏最小二乘判别分析(PLS-DA)能有效判别5个贮藏时间的即食燕窝.依据PLS-DA模型的变量投影重要性分析值(VIP)和指纹图谱结合层次聚类分析,最终筛选出12个(VIP>1)特征挥发性物质,分别为乙酸(单聚体和二聚体)、(Z)-4-庚烯醛、2-丁酮(单聚体)、3-甲基-3-丁烯-1-醇、庚醛、乙酸乙酯(二聚体)、乙酸丙酯(单聚体)、戊醛、丁醛、丙酸乙酯(单聚体和二聚体).通过这些特征化合物可以较好地判别不同贮藏时间的即食燕窝样品.
Analysis of Characteristic Flavor Components of Instant Bird's Nests at Different Storage Time
In order to explore the flavor characteristics of instant bird's nests with different storage times.Gas chromatog-raphy-ion mobility spectroscopy(GC-IMS)was used to analyze the volatile organic compounds of commercial bird's nests at five storage times.The results showed that the volatile components of instant bird's nests varied significantly at differ-ent storage times(P<0.05).A total of 44 volatile organic compounds(including monomers and dimers)were identified,mainly for aldehydes and esters.Principal component analysis(PCA)and partial least squares-discriminant analysis(PLS-DA)could effectively discriminate the instant bird's nests with five storage time.According to the variable impor-tant in the projection(VIP)of PLS-DA model,the results of fingerprint map and hierarchical clustering analysis,12(VIP>1)characteristic volatile substances were finally selected.These characteristic flavor components are acetic acid(M,D),(Z)-hept-4-enal,butan-2-one(M),3-methyl-3-buten-l-ol,heptanal,ethyl acetate(D),propyl acetate(M),pentanal,butanal and propyl acetate(M,D).The samples of instant bird's nests with different storage times can be better discriminated by these characteristic compounds.

gas chromatography-ion mobility spectroscopyinstant bird's nestsprincipal component analysispartial least squares-discriminant analysisvariable important in the projection

林园、张小江、柳训才、黄玉容、熊雅婷、王健

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中国食品发酵工业研究院有限公司 北京 100015

厦门市燕之屋丝浓食品有限公司燕窝研究院 福建厦门 361100

气相色谱-离子迁移谱 即食燕窝 主成分分析 偏最小二乘-判别分析 变量投影重要性分析值

2024

中国食品学报
中国食品科学技术学会

中国食品学报

CSTPCD北大核心EI
影响因子:1.079
ISSN:1009-7848
年,卷(期):2024.24(4)
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