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石吊兰挥发油成分的研究

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目的:研究石吊兰挥发油成分.方法:利用有机溶剂-水蒸气蒸馏法提取石吊兰挥发油,用气相色谱-质谱联用(GC-MS)法进行测定,结合计算机检索技术对分离出的化合物进行结构鉴定,并用色谱峰面积归一化法计算各成分的相对百分含量.结果:分离鉴定出57种化学成分,占挥发油总量的85.334%,其中主要成分及其含量分别为芳樟醇13.935%、l-辛烯-3-醇7.283%、己醛4.172%、苯乙醛3.162%、2-羟基苯甲酸甲基酯2.956%、3-辛醇2.900%、二异丁基邻苯二甲酸酯2.683%、反式-金合欢烯2.607%、香叶基丙酮2.436%、2-正戊基呋喃2.396%、α-松油醇2.393%、反式-2-己烯醛2.228%、六氢假紫罗兰酮2.225%.结论:本文为首次采用 ＧC-MS法对石吊兰挥发油成分进行研究.
Study on Chemical Constituents of Volatile Oil from Lysionotus pauciflorus
OBJECTIVE: To study the chemical constituents of volatile oil from Lysionotus pauciflorus. METHODS: Volatile oil was extracted from L pauciflorus using organic solvent-steam distillation. The chemical constituents of volatile oil were determined by GC-MS. The isolated compounds were identified by computer information retrieval. The relative percentage of chemical constituents was calculated using peak areas normalization. RESULTS: 57 compounds were identified from L. Pauciflorus, accounting for 85.334% of total amount of volatile oil. The contents of main compounds were linalool 13.935% , 1-octen-3-ol 7.283% , hexanal 4.172% , benzeneacetaldehyde 3.162% , 2-hydroxy benzoic acid phenyl methyl ester 2.956% , 3-octanol 2.900% , isobutyl phthalate 2.683% , trans-bata-famesene 2.607% , geranylacetone 2.436% , 2-pentylfuran 2.396% , Alpha-terpineol 2.393% , trans-2-hexenal 2.228%, hexahydropseudoionone 2.225%. CONCLUSION: This is the first time to adopt GC-MS method to study the components of volatile oil from L. Pauciflorus in the study.

Lysionotus pauciflorusOrganic solvent-steam distillationVolatile oilGC-MSAnalysis of constituents

李计龙、刘建华、高玉琼、霍昕、王道平、盛世昌

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贵州大学生命科学院,贵阳市550025

贵州省生物技术研究开发基地,贵阳市550002

贵州省中国科学院天然产物化学重点实验室,贵阳市550009

石吊兰 有机溶剂-水蒸气蒸馏法 挥发油 气相色谱-质谱联用法 成分分析

2011

中国药房
中国医院协会,中国药房杂志社

中国药房

CSTPCDCSCD
影响因子：0.956
ISSN：1001-0408
年,卷(期)：2011.22(27)
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