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聚丙烯输液瓶标准提高研究

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目的:探讨利用差示扫描量热分析方法鉴别聚丙烯输液瓶材料。方法:在氮气氛围下,将样品以20 ℃·min-1速率从40 ℃升至200 ℃后降温至40 ℃,再将样品以10 ℃·min-1速率,从40 ℃升至200 ℃,恒温10 min,再将样品降温至40 ℃以下,绘制其DSC图谱。结果:聚丙烯输液瓶的熔融峰Tm在145~150 ℃之间。结论:该方法准确、灵敏,操作简便,可用于聚丙烯输液瓶材料的鉴别,同时为聚丙烯输液瓶标准提高提供数据参考。
Investigation on improving standard of polypropylene infusion bottles
Objective:To explore the use of differential scanning calorimetry(DSC)method to identify polypropyl-ene infusion bottles material.Methods:The thermal analysis curve under nitrogen was determined at temperatures between 40 ℃ and 200 ℃ with a heating rate of 20 ℃·min-1,then cooled to 40 ℃ at a rate of 20 ℃·min-1.The sample was heated from 40 ℃ to 200 ℃ at a heating rate of 10 ℃·min-1,held the specimen at 200 ℃ for 10 min,then cooled to 40 ℃ at a rate of 10 ℃·min-1.Results:The melting peak temperature(Tm)of polypropyl-ene infusion bottles was between 145-150 ℃.Conclusion:The proposed method is accurate,sensitive,and sim-ple,and can be used for determination of polypropylene infusion bottles material,which can also provide reference for the standard improvement of polypropylene infusion bottles.

polypropyleneinfusion bottlesDSCstandard improvementdeterminationmelting peak

李翔、郑景峰、林芳、徐燕慧、赵霞

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福建省食品药品质量检验研究院,福州 350001

中国食品药品检定研究院,北京 100050

聚丙烯 输液瓶 差示扫描量热分析 标准提高 鉴别 熔融峰

2024

中国药品标准
国家药典委员会

中国药品标准

影响因子:0.372
ISSN:1009-3656
年,卷(期):2024.25(2)