中国药品标准2024,Vol.25Issue(2) :176-180.DOI:10.19778/j.chp.2024.02.011

聚丙烯输液瓶标准提高研究

Investigation on improving standard of polypropylene infusion bottles

李翔 郑景峰 林芳 徐燕慧 赵霞
中国药品标准2024,Vol.25Issue(2) :176-180.DOI:10.19778/j.chp.2024.02.011

聚丙烯输液瓶标准提高研究

Investigation on improving standard of polypropylene infusion bottles

李翔 1郑景峰 1林芳 1徐燕慧 1赵霞2
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作者信息

  • 1. 福建省食品药品质量检验研究院,福州 350001
  • 2. 中国食品药品检定研究院,北京 100050
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摘要

目的:探讨利用差示扫描量热分析方法鉴别聚丙烯输液瓶材料.方法:在氮气氛围下,将样品以20 ℃·min-1速率从40 ℃升至200 ℃后降温至40 ℃,再将样品以10 ℃·min-1速率,从40 ℃升至200 ℃,恒温10 min,再将样品降温至40 ℃以下,绘制其DSC图谱.结果:聚丙烯输液瓶的熔融峰Tm在145~150 ℃之间.结论:该方法准确、灵敏,操作简便,可用于聚丙烯输液瓶材料的鉴别,同时为聚丙烯输液瓶标准提高提供数据参考.

Abstract

Objective:To explore the use of differential scanning calorimetry(DSC)method to identify polypropyl-ene infusion bottles material.Methods:The thermal analysis curve under nitrogen was determined at temperatures between 40 ℃ and 200 ℃ with a heating rate of 20 ℃·min-1,then cooled to 40 ℃ at a rate of 20 ℃·min-1.The sample was heated from 40 ℃ to 200 ℃ at a heating rate of 10 ℃·min-1,held the specimen at 200 ℃ for 10 min,then cooled to 40 ℃ at a rate of 10 ℃·min-1.Results:The melting peak temperature(Tm)of polypropyl-ene infusion bottles was between 145-150 ℃.Conclusion:The proposed method is accurate,sensitive,and sim-ple,and can be used for determination of polypropylene infusion bottles material,which can also provide reference for the standard improvement of polypropylene infusion bottles.

关键词

聚丙烯/输液瓶/差示扫描量热分析/标准提高/鉴别/熔融峰

Key words

polypropylene/infusion bottles/DSC/standard improvement/determination/melting peak

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出版年

2024
中国药品标准
国家药典委员会

中国药品标准

影响因子:0.372
ISSN:1009-3656
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