Comparison the Content s of Heavy Metals and Harmful Elements in Dioscoreae Rhizoma by ICP-MS
Objective:To compare the contents of five heavy metals and harmful elements(Cu,Pb,As,Cd and Hg)in Maoshanyao and Guangshanyao.Methods:The sample solution was prepared by microwave digestion,and the contents of Cu,Pb,As,Cd and Hg were determined by inductively coupled plasma mass spectrometry(ICP-MS)with Germanium,indium and bismuth as internal standard.Results:The linear relationships of Cu,Pb,As,Cd and Hg were good(r≥0.999 5),and the recoveries were 82.4%-103.6%.RSD range was 2.4%to 5.9%.The content determination results showed that compared with Maoshanyao,the content of five heavy metals and harmful elements in Guangshanyao significantly decreased,and the proportion of copper residue reduction was 60.41%-73.57%.Conclusion:Compared with Maoshanyao,Guangshanyao contains lower levels of heavy metals and harmful elements residues.
Dioscoreae RhizomaMaoshanyaoGuangshanyaoHeavy metals and harmful elementsInductively coupled plasma mass spectrometry(ICP-MS)