中国药学杂志1999,Issue(4) :262.

复方木鸡口服液质量标准的研究

Quality standard of compound mujian koufuye

王红燕 车东 缪桂凤 罗贵华
中国药学杂志1999,Issue(4) :262.

复方木鸡口服液质量标准的研究

Quality standard of compound mujian koufuye

王红燕 1车东 2缪桂凤 2罗贵华3
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作者信息

  • 1. 沈阳110015沈阳药科大学
  • 2. 丹东118002丹东中药厂
  • 3. 天津300171天津制药厂
  • 折叠

摘要

目的:为控制复方木鸡口服液的质量,建立山豆根、核桃楸皮的薄层色谱鉴别及苦参碱的薄层扫描定量方法。方法:将样品中的山豆根与核桃楸皮进行薄层鉴别。对山豆根中的苦参碱进行薄层扫描定量。结果:鉴别方法专属性强,定量方法简便、准确,平均回收率为102.0%,RSD为4.78%。结论:本质量标准可有效地控制复方木鸡口服液的质量。

Abstract

OBJECTIVE:To estabolish the quality control of Compound Mujian Koufuye:the TLC identification method of Sophora subprostrata and Juglans mandshurica and the quantitative determination of matrine by TLCS.METHODS:The sample was identified respectively by TLC in contrast with Sophora subprostrata and Juglans mandshurica drugs after it was pretreated.,Matrine in Compound Mujian Koufuye was extracted refluxently with CHCl3 and determined by the dual wavelength thin layer chromatography scanning.RESULTS:The TLC identification was highly specific and the spots were clear and concentrated.The quantitative method was simple,sensitive,reproducible and accurate.The average recovery of matrine in the sample was 102.0%(n=5).The relative standard deviation was 4.78%.CONCLUSION:The quality standard was able to effectively control the quality of Compound Mujian Koufuye.

关键词

复方木鸡口服液/山豆根/核桃楸皮/苦参碱/薄层扫描

Key words

Compound Muian Koufuye,Sophora subprostrata,Juglans mandshurica,matrine,TLCS

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出版年

1999
中国药学杂志
中国药学会

中国药学杂志

CSCD北大核心
影响因子:0.957
ISSN:1001-2494
被引量3
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