首页|ICP-AES法分析硫磺熏蒸前后白芍中有害重金属、硫及主要微量元素的变化

ICP-AES法分析硫磺熏蒸前后白芍中有害重金属、硫及主要微量元素的变化

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目的:进行硫磺熏蒸前后白芍样品中有害重金属、硫及微量元素的分析.方法:采用湿法消解前处理,电感耦合等离子发射光谱(ICP-AES)法测定.结果:白芍经硫磺熏蒸后Cu,S元素含量增加,Zn元素含量降低,并且在硫磺熏蒸白芍样品中检测到了重金属As,Hg残留.结论:硫磺熏蒸可能会使白芍中残留有害重金属及大量对人体有危害的硫,同时改变部分微量元素的含量.
Analysis of harmful heavy metals, sulfur and main trace elements from Paeoniae Radix Alba before and after sulfur-fumigated process by ICP-AES method
Objective; To analyze the contents of harmful heavy metals, sulfur and trace elements from Paeoniae Radix Alba before and after sulfur-fumigated process. Method: Samples were pretreated by wet digestion and then subjected to elements analysis by inductively coupled plasma-atomic emission spectrometry (ICP-AES). Result; The contents of Cu and S elements were increased, while the content of Zn element was decreased in Paeoniae Radix Alba after sulfur-fumigated process compared with the samples dried in the sun. Moreover, heavy metallic elements, such as As and Hg, were detected in Paeoniae Radix Alba after sulfur-fumigated process. Conclusion; Sulfur fumigated process may cause residual of heavy metals and sulfur which are harmful to human body and change the contents of some trace elements.

Paeoniae Radix Albasulfur-fumigated processharmful heavy metalssulfurtrace elementsICP-AES

刘静静、蔡皓、刘晓、马晓青、李松林、宗杜强、蔡宝昌

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南京中医药大学药学院,江苏南京,210046

南京中医药大学国家教育部中药炮制规范化及标准化工程研究中心,江苏南京,210029

南京中医药大学国家中医药管理局中药炮制标准重点研究室,江苏南京,210029

南京海昌中药集团,江苏南京,210061

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白芍 硫磺熏蒸 有害重金属 微量元素 电感耦合等离子发射光谱

国家自然科学基金江苏省自然科学基金

30940093BK2009495

2011

中国中药杂志
中国药学会

中国中药杂志

CSTPCDCSCD北大核心
影响因子:1.718
ISSN:1001-5302
年,卷(期):2011.36(13)
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