首页|凝脂莲香精成分分析及最优提取方式研究

凝脂莲香精成分分析及最优提取方式研究

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提取景天科Crassulaceae植物凝脂莲Sedum clavatum的香精成分,并分析不同部位香精组分差异性,提高凝脂莲香精提取的产量.采用微波辅助水蒸气法提取植株、叶片以及茎秆部位的香精,气相色谱-质谱联用技术分析凝脂莲植株、叶片与茎秆香精的成分,通过单因素实验探求香精提取的最佳条件,正交实验筛选最优条件组合.研究发现茎秆部位提取率大约为叶片部位提取率的4倍,茎秆香精与植株香精成分重复物质为2种,占植株香精成分的 16.91%.实验结果表明,在固液比 1:8、浸泡时间 60 min、微波功率 400 W、提取时间 3 h的条件下,提取率最高,最高提取率为 0.96%.
The Optimal Technology for Extraction of Essential Oil and Analysis on Its Components from Sedum clavatum
Extraction of essential oil from the whole plant,leaves and stem of Sedum clavatum was implemented by microwave assisted hydro-distillation,and analysis were made on their component by gas chromatography-mass spectrometry.The optimal technology for extraction was experimented with single factor and orthogonal design.The result demonstrated that the extraction rate of essential oil from stem was about 4 times higher than that from leaf,and there were 2 same substances in essential oil from stem and the whole plant.The experiment showed the optimal technology for extraction of essential oil from different part of S.clavatum was as follows:solid-liquid ratio of 1:8,soaking time of 60 min,microwave power of 400 W,and extraction time of 3 h,the highest extraction rate reached 0.96%.

Sedum clavatummicrowave assisted hydro distillationessential oilgas chromatography-mass spectrometrysingle factor experimentorthogonal test

陶厚璜、周泓彬、郭明

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浙江农林大学 化学与材料工程学院,浙江 杭州 311300

凝脂莲 微波辅助水蒸气法 香精 气相色谱-质谱联用 单因素实验 正交试验

浙江省公益基金

LGN20B070001

2024

浙江林业科技
浙江省林业科学研究院 浙江省林学会 浙江省林业科技情报中心

浙江林业科技

影响因子:0.483
ISSN:1001-3776
年,卷(期):2024.44(1)
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