浙江林业科技2024,Vol.44Issue(1) :25-32.DOI:10.3969/j.issn.1001-3776.2024.01.004

凝脂莲香精成分分析及最优提取方式研究

The Optimal Technology for Extraction of Essential Oil and Analysis on Its Components from Sedum clavatum

陶厚璜 周泓彬 郭明
浙江林业科技2024,Vol.44Issue(1) :25-32.DOI:10.3969/j.issn.1001-3776.2024.01.004

凝脂莲香精成分分析及最优提取方式研究

The Optimal Technology for Extraction of Essential Oil and Analysis on Its Components from Sedum clavatum

陶厚璜 1周泓彬 1郭明1
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作者信息

  • 1. 浙江农林大学 化学与材料工程学院,浙江 杭州 311300
  • 折叠

摘要

提取景天科Crassulaceae植物凝脂莲Sedum clavatum的香精成分,并分析不同部位香精组分差异性,提高凝脂莲香精提取的产量.采用微波辅助水蒸气法提取植株、叶片以及茎秆部位的香精,气相色谱-质谱联用技术分析凝脂莲植株、叶片与茎秆香精的成分,通过单因素实验探求香精提取的最佳条件,正交实验筛选最优条件组合.研究发现茎秆部位提取率大约为叶片部位提取率的4倍,茎秆香精与植株香精成分重复物质为2种,占植株香精成分的 16.91%.实验结果表明,在固液比 1:8、浸泡时间 60 min、微波功率 400 W、提取时间 3 h的条件下,提取率最高,最高提取率为 0.96%.

Abstract

Extraction of essential oil from the whole plant,leaves and stem of Sedum clavatum was implemented by microwave assisted hydro-distillation,and analysis were made on their component by gas chromatography-mass spectrometry.The optimal technology for extraction was experimented with single factor and orthogonal design.The result demonstrated that the extraction rate of essential oil from stem was about 4 times higher than that from leaf,and there were 2 same substances in essential oil from stem and the whole plant.The experiment showed the optimal technology for extraction of essential oil from different part of S.clavatum was as follows:solid-liquid ratio of 1:8,soaking time of 60 min,microwave power of 400 W,and extraction time of 3 h,the highest extraction rate reached 0.96%.

关键词

凝脂莲/微波辅助水蒸气法/香精/气相色谱-质谱联用/单因素实验/正交试验

Key words

Sedum clavatum/microwave assisted hydro distillation/essential oil/gas chromatography-mass spectrometry/single factor experiment/orthogonal test

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基金项目

浙江省公益基金(LGN20B070001)

出版年

2024
浙江林业科技
浙江省林业科学研究院 浙江省林学会 浙江省林业科技情报中心

浙江林业科技

影响因子:0.483
ISSN:1001-3776
参考文献量9
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