首页|氧化锌纳米复合材料的场发射性能研究

氧化锌纳米复合材料的场发射性能研究

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采用两步法制备得到氧化锌纳米复合材料.首先采用低温水热法在硅基底上生长得到氧化锌纳米棒阵列,再采用电泳法分别制备得到 3 种氧化锌纳米复合材料,并对所得产物进行了 SEM、XRD、EDS和 XPS表征,最后对产物进行了场发射性能测试.XRD、EDS和XPS测试结果表明制备产物为Al2O3-ZnO、MgO-ZnO和CuO-ZnO纳米复合材料.同氧化锌纳米棒阵列相比,3 种氧化锌纳米复合样品的开启电场均有所下降,其中 MgO-ZnO 纳米复合样品的场发射性能最优,开启电场为4.7 V/μm,4 种样品的开启电场从低到高依次是:MgO-ZnO<Al2O3-ZnO<CuO-ZnO<ZnO,研究结果表明构建纳米复合材料能够有效提高氧化锌纳米棒的场发射性能.
Investigation on Field Emission Performance of Zinc Oxide Nanocomposites
Zinc oxide nanocomposites are prepared using a two-step method.Firstly,ZnO nanorod ar-rays are grown on a silicon substrate by a low-temperature hydrothermal method.Then three types of zinc oxide nanocomposites are obtained using electrophoresis method.All products are characterized by SEM,XRD,EDS,XPS,and finally the field emission performances of the products are investigated.The results of XRD,EDS,and XPS characterizations indicate that the prepared products are Al2O3-ZnO,MgO-ZnO,and CuO-ZnO nanocomposites.Compared with pristine ZnO nanorods,the three ZnO nanocomposite sam-ples all have lower turn on fields.The MgO-ZnO nanocomposite sample exhibits the best field emission performance,with a turn-on field of 4.7 V/μm.The turn-on fields of the four samples,from low to high,are as follows:MgO-ZnO<Al2O3-ZnO<CuO-ZnO<ZnO.The results suggest that the construction of nanocomposites can effectively improve the field emission performance of ZnO nanorods.

Field emissionZnO nanorodsNanocomposite materialHydrothermal methodElectro-phoresis

陈贵滔、钱维金、涂友情、黄卫军、董长昆

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温州大学 温州市微纳光电器件重点实验室,浙江 温州 325035

场发射 氧化锌纳米棒 纳米复合材料 水热法 电泳法

2024

真空电子技术
北京真空电子技术研究所

真空电子技术

影响因子:0.166
ISSN:1002-8935
年,卷(期):2024.(4)