首页|荔枝核多酚类物质的分离与鉴定

荔枝核多酚类物质的分离与鉴定

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  • 国家科技期刊平台
  • NETL
  • NSTL
  • 万方数据
  • 维普
目的:研究荔枝核的多酚类物质成分.方法:采用65%乙醇提取荔枝核,经系统溶剂萃取后,用硅胶柱色谱、聚酰胺柱色谱以及制备薄层色谱进行分离纯化,根据理化性质和波谱分析鉴定化合物的结构.结果:从荔枝核乙酸乙酯萃取物中分离鉴定了4个多酚类化合物,分别为原儿茶醛(Ⅰ)、原儿茶酸(Ⅱ)、胡萝卜苷(Ⅲ)和(-)-表儿茶素(Ⅳ).结论:其中化合物Ⅰ、Ⅲ、Ⅳ为首次从该植物中分离得到.
Isolation and Characterization of Polyphenols in Seed of Litchi chinensis
Objective: To study the chemical constituents of polyphenols in seed of Litchi chinensis. Methods: The seeds of Litchi chinensis were extracted by 65% ethanol, then the compounds were separated by repeated silica gel, polyamide and preparative TLC. The structures of polyphones isolated were identified by analysis of their spectral datas and chemical properties. Results: Four poly-phones compounds were isolated as protocatechuic aldehyde ( Ⅰ ), protocatechuic acid ( Ⅱ ), daucosterol ( Ⅲ ) and ( - ) -epicatichin (Ⅳ). Conclusions: Compounds Ⅰ , Ⅲ and Ⅳ are isolated from this plant for the first time.

Seed of Litchi chinensisProtocatechuic aldehydeProtocatechuic acidDaucosterol( - ) -epicatichin

颜仁梁、刘志刚

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广东省食品药品职业学院,广东,广州510520

广州军区广州总医院药学部,广东,广州510010

广州中医药大学,广东,广州510405

荔枝核 原儿茶醛 原儿茶酸 胡萝卜苷 (-)-表儿茶素

2009

中药材
国家食品药品监督管理局,中药材信息中心站

中药材

CSTPCDCSCD北大核心
影响因子：0.913
ISSN：1001-4454
年,卷(期)：2009.32(4)
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