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GC测定强龙益肾胶囊中丁香酚含量

Dertermination of Eugenol in Qianglong Yishen Capsule by GC

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目的:建立测定强龙益肾胶囊中丁香酚含量的气相色谱法.方法:Agilent DB-WAX(30.0m×0.53mm,1.00μm)毛细管柱,火焰离子化检测器(FID),以氮气为载气,柱温210℃,进样口温度220℃,检测器温度250℃.分流比5:1.结果:丁香酚在0.01321-0.42272μg线性关系良好,r=0.9994,平均加样回收率为98.31%.RSD为0.95%.结论:该方法操作简便,结果准确、可靠,可用于该制剂的质量控制.
Objective: To establish a GC method for determination of Eugenol in Qianglong Yishen Capsule.Methods:The analysis was performed on capillary column of Agilent DB -WAX (30.0m × 0.53 mm, 1.00μm) ,with FID detector,using nitrogen as carrier gas.The column temperature was 210℃ ,The injector temperature was set at 220℃ and the detector temperature was 250℃.The split ratio was 5 : 1.Results: The linearity was good for Eugenol within the range of 0.01321 ~0.42272μg, r =0.999 4,The average recovery of butanone was 98.31% ,RSD =0.95%.Conclusion: The method is simple ,rapid,accurate and can be used to control the quality of Qianglong Yishen capsule.

Qianglong Yishen CapsuleeugenolGC

朱克、蒋士鹏、周玲娜

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浙江省金华市食品药品检验所,浙江金华,321000

丁香酚 强龙益肾胶囊 气相色谱法 含量

2011

中华中医药学刊
中华中医药学会 ,辽宁中医药大学

中华中医药学刊

CSTPCD
影响因子:1.007
ISSN:1673-7717
年,卷(期):2011.29(5)
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